iPrOC₆H₃(CHCH₂)O(CH₂)4C₃H₃N₂MesCl

Base Information

• Chemical Name: iPrOC₆H₃(CHCH₂)O(CH₂)4C₃H₃N₂MesCl
• CAS No.: 1056474-08-8
• Molecular Formula: C₂₇H₃₅N₂O₂*Cl
• Molecular Weight: 455.04
• Mol file: 1056474-08-8.mol

Synonyms:iPrOC₆H₃(CHCH₂)O(CH₂)4C₃H₃N₂MesCl

Chemical Property of iPrOC₆H₃(CHCH₂)O(CH₂)4C₃H₃N₂MesCl

Chemical Property:

Purity/Quality:

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Technology Process of iPrOC₆H₃(CHCH₂)O(CH₂)4C₃H₃N₂MesCl

There total 1 articles about iPrOC₆H₃(CHCH₂)O(CH₂)4C₃H₃N₂MesCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.5%

N-(2,4,6-trimethylphenyl)imidazole (25364-44-7) + 5-(4-chlorobutoxy)-2-isopropoxystyrene (607364-51-2) → iPrOC6H3(CHCH2)O(CH2)4C3H3N2MesCl (1056474-08-8)

Guidance literature:

In toluene; at 100 - 110 ℃; for 48h;

DOI:10.1039/b809025d

Reference yield: 60.0%

Grubbs catalyst first generation + iPrOC6H3(CHCH2)O(CH2)4C3H3N2MesCl (1056474-08-8) → (iPrOC6H3(CHCH2)O(CH2)4C3H2N2Mes)RuCl2(CHPh)(PCy3)

Guidance literature:

With potassium tert-butylate; In toluene; treatment of toluene soln. of imidazolium compd. with potassium tert-butoxide and then with ruthenium compd. at 0°C, stirring for 3 h under N2 at room temp.; filtration, evapn., chromy. (silica gel, ethyl acetate/hexane (1:3)), NMR;

DOI:10.1039/b809025d

upstream raw materials:

N-(2,4,6-trimethylphenyl)imidazole

5-(4-chlorobutoxy)-2-isopropoxystyrene