(η6-1-triphenylstannylbenzene)(η5-cyclopentadienyl)iron(II) hexafluorophosphate

Base Information

Chemical Name:(η6-1-triphenylstannylbenzene)(η5-cyclopentadienyl)iron(II) hexafluorophosphate
CAS No.:108089-23-2
Molecular Formula:C₂₉H₂₅FeSn*F₆P
Molecular Weight:693.039
Hs Code.:

Synonyms:(η6-1-triphenylstannylbenzene)(η5-cyclopentadienyl)iron(II) hexafluorophosphate

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Chemical Property of (η6-1-triphenylstannylbenzene)(η5-cyclopentadienyl)iron(II) hexafluorophosphate

Chemical Property:

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Technology Process of (η6-1-triphenylstannylbenzene)(η5-cyclopentadienyl)iron(II) hexafluorophosphate

There total 1 articles about (η6-1-triphenylstannylbenzene)(η5-cyclopentadienyl)iron(II) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.7%

: ammonium hexafluorophosphate

: 4167-90-2
triphenylstannyllithium

: (η6-chlorobenzene)(η5-cyclopentadienyl)iron(II) hexafluorophosphate

: 108089-23-2
(η6-1-triphenylstannylbenzene)(η5-cyclopentadienyl)iron(II) hexafluorophosphate

Guidance literature:: In tetrahydrofuran; byproducts: LiCl; (N2); soln. of Ph3SnLi added via a syringe at -78°C; allowed to warm to room temp.; left for 60 h with stirring; quenched with NH4PF6 at0°C; THF evapd. off; extd. (acetone); evapd.; recrystd. (methanol); elem. anal.;
DOI:10.1016/0022-328X(86)80476-4

Reference yield: 45.0%

: 108089-23-2
(η6-1-triphenylstannylbenzene)(η5-cyclopentadienyl)iron(II) hexafluorophosphate

: mercury dichloride

: (η6-diphenyliodostannylbenzene)(η5-cyclopentadienyl)iron(II) tetraiodomercurate

: 100-56-1
phenylmercury(II) chloride

Guidance literature:: With KI; In acetone; byproducts: [(C5H5)Fe(C6H5)Sn(C6H5)2Cl)]PF6; ((C5H5)Fe(C6H5)Sn(C6H5)3)PF6 in acetone is added to HgCl2 in acetone; refluxed briefly; cooled to -5°C, filtered off; filtrate added to a soln. of KI; excess HgCl2 removed; ppt. filtered off; elem. anal.; IR;
DOI:10.1016/0022-328X(86)80476-4

Reference yield: 42.0%

: 108089-23-2
(η6-1-triphenylstannylbenzene)(η5-cyclopentadienyl)iron(II) hexafluorophosphate

: 108089-26-5
(η6-diphenyliodostannylbenzene)(η5-cyclopentadienyl)iron(II) iodide

Guidance literature:: With I₂; In acetone; refluxed for 5 min; cooled; added to ether, filtered off; dried (air); elem. anal.; IR;
DOI:10.1016/0022-328X(86)80476-4