allyl 2-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-6-O-(4-methoxyphenyl)-α-D-glucopyranoside

Base Information

• Chemical Name: allyl 2-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-6-O-(4-methoxyphenyl)-α-D-glucopyranoside
• CAS No.: 1343987-86-9
• Molecular Formula: C₈₄H₉₀O₁₇
• Molecular Weight: 1371.63

Synonyms:allyl 2-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-6-O-(4-methoxyphenyl)-α-D-glucopyranoside

Chemical Property of allyl 2-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-6-O-(4-methoxyphenyl)-α-D-glucopyranoside

Chemical Property:

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Technology Process of allyl 2-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-6-O-(4-methoxyphenyl)-α-D-glucopyranoside

There total 1 articles about allyl 2-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-6-O-(4-methoxyphenyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

C89H98O18 (1343988-85-1) → allyl 2-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-6-O-(4-methoxyphenyl)-α-D-glucopyranoside (1343987-86-9)

Guidance literature:

With methanol; sodium methylate; In tetrahydrofuran; at 20 ℃; for 42h;

Reference yield: 73.0%

allyl 2-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-6-O-(4-methoxyphenyl)-α-D-glucopyranoside (1343987-86-9) + benzyl bromide (100-39-0) → C91H96O17 (1343987-89-2)

Guidance literature:

allyl 2-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-6-O-(4-methoxyphenyl)-α-D-glucopyranoside; With sodium hydride; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; mineral oil; at 0 ℃;

benzyl bromide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; mineral oil; at 20 ℃; for 18h;

Reference yield:

3,4,6-tri-O-acetyl-2-azido-2-deoxy-α/β-D-glucopyranosyl trichloroacetimidate (1330067-77-0) + allyl 2-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-6-O-(4-methoxyphenyl)-α-D-glucopyranoside (1343987-86-9) → C101H109N3O23

Guidance literature:

3,4,6-tri-O-acetyl-2-azido-2-deoxy-α/β-D-glucopyranosyl trichloroacetimidate; allyl 2-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-6-O-(4-methoxyphenyl)-α-D-glucopyranoside; In diethyl ether; for 0.166667h; AW-300 molecular sieves;

With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; dichloromethane; at 0 ℃; for 0.75h;

upstream raw materials:

C₈₉H₉₈O₁₈

Downstream raw materials:

C₉₁H₉₆O₁₇

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