N-benzyloxycarbonyl-L-phenylalanyl-1-amino-3-(benzyloxy)-methoxypropan-2-one

Base Information

Chemical Name:N-benzyloxycarbonyl-L-phenylalanyl-1-amino-3-(benzyloxy)-methoxypropan-2-one
CAS No.:174537-41-8
Molecular Formula:C₂₈H₃₀N₂O₆
Molecular Weight:490.556
Hs Code.:

Synonyms:N-benzyloxycarbonyl-L-phenylalanyl-1-amino-3-(benzyloxy)-methoxypropan-2-one

Suppliers and Price of N-benzyloxycarbonyl-L-phenylalanyl-1-amino-3-(benzyloxy)-methoxypropan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyloxycarbonyl-L-phenylalanyl-1-amino-3-(benzyloxy)-methoxypropan-2-one

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N-benzyloxycarbonyl-L-phenylalanyl-1-amino-3-(benzyloxy)-methoxypropan-2-one

There total 6 articles about N-benzyloxycarbonyl-L-phenylalanyl-1-amino-3-(benzyloxy)-methoxypropan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: N-benzyloxycarbonyl-L-phenylalanyl-1-amino-3-(benzyloxy)-methoxypropan-2-ol

: 174537-41-8
N-benzyloxycarbonyl-L-phenylalanyl-1-amino-3-(benzyloxy)-methoxypropan-2-one

Guidance literature:: With Dess-Martin periodane; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1016/0223-5234(96)88312-7

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 174537-41-8
N-benzyloxycarbonyl-L-phenylalanyl-1-amino-3-(benzyloxy)-methoxypropan-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 56 percent / ethyldiisopropylamine / CHCl₃ / Ambient temperature

2: 2.76 g / NH₃ / ethanol / 72 h / Ambient temperature

3: tetrahydrofuran / 2 h / -15 °C

4: 52 percent / periodinane / CH₂Cl₂ / 2 h / Ambient temperature

With ammonia; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane; chloroform;
DOI:10.1016/0223-5234(96)88312-7

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 174537-41-8
N-benzyloxycarbonyl-L-phenylalanyl-1-amino-3-(benzyloxy)-methoxypropan-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: N-methylmorpholine / tetrahydrofuran / 0.5 h / -15 °C

2: tetrahydrofuran / 2 h / -15 °C

3: 52 percent / periodinane / CH₂Cl₂ / 2 h / Ambient temperature

With 4-methyl-morpholine; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;
DOI:10.1016/0223-5234(96)88312-7