(3S) 3,7-Dibenzyl-3,4-dihydro-4-methyl-2H-1,4-diazepino<6,5-c>chinolin-2,5(1H)-dion

Base Information

Chemical Name:(3S) 3,7-Dibenzyl-3,4-dihydro-4-methyl-2H-1,4-diazepino<6,5-c>chinolin-2,5(1H)-dion
CAS No.:114700-32-2
Molecular Formula:C₂₇H₂₃N₃O₂
Molecular Weight:421.499
Hs Code.:

Synonyms:(3S) 3,7-Dibenzyl-3,4-dihydro-4-methyl-2H-1,4-diazepino<6,5-c>chinolin-2,5(1H)-dion

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Chemical Property of (3S) 3,7-Dibenzyl-3,4-dihydro-4-methyl-2H-1,4-diazepino<6,5-c>chinolin-2,5(1H)-dion

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Technology Process of (3S) 3,7-Dibenzyl-3,4-dihydro-4-methyl-2H-1,4-diazepino<6,5-c>chinolin-2,5(1H)-dion

There total 6 articles about (3S) 3,7-Dibenzyl-3,4-dihydro-4-methyl-2H-1,4-diazepino<6,5-c>chinolin-2,5(1H)-dion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 114700-29-7
(3S,11bS) 3,7-Dibenzyl-3,4,7,11b-tetrahydro-4-methyl-2H-1,4-diazepino<6,5-c>chinolin-2,5(1H)-dion

: 114700-32-2
(3S) 3,7-Dibenzyl-3,4-dihydro-4-methyl-2H-1,4-diazepino<6,5-c>chinolin-2,5(1H)-dion

Guidance literature:: With potassium tert-butylate; chloranil; In dichloromethane; Heating;

Reference yield:

: 84741-86-6
quinoline-3-carbonyl chloride

: 114700-32-2
(3S) 3,7-Dibenzyl-3,4-dihydro-4-methyl-2H-1,4-diazepino<6,5-c>chinolin-2,5(1H)-dion

Guidance literature:: Multi-step reaction with 5 steps

1: 50 percent

2: 72 percent / NH₃ / methanol / 12 h

3: 84 percent

4: 1.) KOH / 1.) H₂O, CH₂Cl₂, 2.) CH₂Cl₂, reflux, 24 h

5: 18 percent / chloranil, t-BuOK / CH₂Cl₂ / Heating

With potassium hydroxide; potassium tert-butylate; ammonia; chloranil; In methanol; dichloromethane;

Reference yield:

: 2812-24-0
(S)-ethyl-2-(methylamino)-3-phenylpropanoate

: 114700-32-2
(3S) 3,7-Dibenzyl-3,4-dihydro-4-methyl-2H-1,4-diazepino<6,5-c>chinolin-2,5(1H)-dion

Guidance literature:: Multi-step reaction with 5 steps

1: 50 percent

2: 72 percent / NH₃ / methanol / 12 h

3: 84 percent

4: 1.) KOH / 1.) H₂O, CH₂Cl₂, 2.) CH₂Cl₂, reflux, 24 h

5: 18 percent / chloranil, t-BuOK / CH₂Cl₂ / Heating

With potassium hydroxide; potassium tert-butylate; ammonia; chloranil; In methanol; dichloromethane;