3-[(p-nitrophenyl)methoxy]-2,2-dimethyl-1-propanol-[p-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl) benzoate]

Base Information

• Chemical Name: 3-[(p-nitrophenyl)methoxy]-2,2-dimethyl-1-propanol-[p-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl) benzoate]
• CAS No.: 548776-79-0
• Molecular Formula: C₂₅H₃₂BNO₇
• Molecular Weight: 469.343

Synonyms:3-[(p-nitrophenyl)methoxy]-2,2-dimethyl-1-propanol-[p-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl) benzoate]

Chemical Property of 3-[(p-nitrophenyl)methoxy]-2,2-dimethyl-1-propanol-[p-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl) benzoate]

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Technology Process of 3-[(p-nitrophenyl)methoxy]-2,2-dimethyl-1-propanol-[p-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl) benzoate]

There total 3 articles about 3-[(p-nitrophenyl)methoxy]-2,2-dimethyl-1-propanol-[p-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl) benzoate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

4-carboxyphenylboronic acid pinacol ester (180516-87-4) + 3-[(p-nitrophenyl)methoxy]-2,2-dimethyl-1-propanol (548776-78-9) → 3-[(p-nitrophenyl)methoxy]-2,2-dimethyl-1-propanol-[p-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl) benzoate] (548776-79-0)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃;

DOI:10.1071/CH02267

Reference yield:

2,2-Dimethyl-1,3-propanediol (126-30-7) → 3-[(p-nitrophenyl)methoxy]-2,2-dimethyl-1-propanol-[p-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl) benzoate] (548776-79-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 43 percent / Ag₂O / CH₂Cl₂ / 24 h / 20 °C

2: 68 percent / DMAP; DCC / CH₂Cl₂ / 0 - 20 °C

With dmap; dicyclohexyl-carbodiimide; silver(l) oxide; In dichloromethane;

DOI:10.1071/CH02267

Reference yield:

1-bromomethyl-4-nitro-benzene (100-11-8) → 3-[(p-nitrophenyl)methoxy]-2,2-dimethyl-1-propanol-[p-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl) benzoate] (548776-79-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 43 percent / Ag₂O / CH₂Cl₂ / 24 h / 20 °C

2: 68 percent / DMAP; DCC / CH₂Cl₂ / 0 - 20 °C

With dmap; dicyclohexyl-carbodiimide; silver(l) oxide; In dichloromethane;

DOI:10.1071/CH02267

upstream raw materials:

4-carboxyphenylboronic acid pinacol ester

3-[(p-nitrophenyl)methoxy]-2,2-dimethyl-1-propanol

2,2-Dimethyl-1,3-propanediol

1-bromomethyl-4-nitro-benzene

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