N₂-(2-isopropoxy-5-methyl-4-(1-methylpiperidin-4-yl)phenyl)-N₄-(2-(isopropylsulfonyl)phenyl)pyrazolo[1,5-a][1,3,5]triazine-2,4-diamine

Base Information

• Chemical Name: N₂-(2-isopropoxy-5-methyl-4-(1-methylpiperidin-4-yl)phenyl)-N₄-(2-(isopropylsulfonyl)phenyl)pyrazolo[1,5-a][1,3,5]triazine-2,4-diamine
• CAS No.: 1190115-51-5
• Molecular Formula: C₃₀H₃₉N₇O₃S
• Molecular Weight: 577.751

Synonyms:N₂-(2-isopropoxy-5-methyl-4-(1-methylpiperidin-4-yl)phenyl)-N₄-(2-(isopropylsulfonyl)phenyl)pyrazolo[1,5-a][1,3,5]triazine-2,4-diamine

Chemical Property of N₂-(2-isopropoxy-5-methyl-4-(1-methylpiperidin-4-yl)phenyl)-N₄-(2-(isopropylsulfonyl)phenyl)pyrazolo[1,5-a][1,3,5]triazine-2,4-diamine

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Technology Process of N₂-(2-isopropoxy-5-methyl-4-(1-methylpiperidin-4-yl)phenyl)-N₄-(2-(isopropylsulfonyl)phenyl)pyrazolo[1,5-a][1,3,5]triazine-2,4-diamine

There total 2 articles about N₂-(2-isopropoxy-5-methyl-4-(1-methylpiperidin-4-yl)phenyl)-N₄-(2-(isopropylsulfonyl)phenyl)pyrazolo[1,5-a][1,3,5]triazine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-isopropoxy-5-methyl-4-(1-methyl-piperidin-4-yl)-phenylamine (1032903-66-4) + N-(2-(isopropylsulfonyl)phenyl)-2-(methylsulfonyl)pyrazolo[1,5-a][1,3,5]triazine (1190115-53-7) → N2-(2-isopropoxy-5-methyl-4-(1-methylpiperidin-4-yl)phenyl)-N4-(2-(isopropylsulfonyl)phenyl)pyrazolo[1,5-a][1,3,5]triazine-2,4-diamine (1190115-51-5)

Guidance literature:

With toluene-4-sulfonic acid; In isopropyl alcohol; at 150 ℃; for 3h;

Reference yield:

N-(2-(isopropylsulfonyl)phenyl)-2-(methylthio)pyrazolo[1,5-a][1,3,5]triazine (1190115-52-6) → N2-(2-isopropoxy-5-methyl-4-(1-methylpiperidin-4-yl)phenyl)-N4-(2-(isopropylsulfonyl)phenyl)pyrazolo[1,5-a][1,3,5]triazine-2,4-diamine (1190115-51-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / 1,2-dichloro-ethane / 0 - 20 °C

2: toluene-4-sulfonic acid / isopropyl alcohol / 3 h / 150 °C

With toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In 1,2-dichloro-ethane; isopropyl alcohol;

upstream raw materials:

2-isopropoxy-5-methyl-4-(1-methyl-piperidin-4-yl)-phenylamine

N-(2-(isopropylsulfonyl)phenyl)-2-(methylsulfonyl)pyrazolo[1,5-a][1,3,5]triazine

N-(2-(isopropylsulfonyl)phenyl)-2-(methylthio)pyrazolo[1,5-a][1,3,5]triazine

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