2ξ-(2,6-dimethoxybenzoyl)-2ξ,3ξ-epoxy-3ξ-methoxycarbonyl-7-oxabicyclo<2.2.1>heptane

Base Information

Chemical Name:2ξ-(2,6-dimethoxybenzoyl)-2ξ,3ξ-epoxy-3ξ-methoxycarbonyl-7-oxabicyclo<2.2.1>heptane
CAS No.:76505-13-0
Molecular Formula:C₁₇H₁₈O₇
Molecular Weight:334.326
Hs Code.:

Synonyms:2ξ-(2,6-dimethoxybenzoyl)-2ξ,3ξ-epoxy-3ξ-methoxycarbonyl-7-oxabicyclo<2.2.1>heptane

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Chemical Property of 2ξ-(2,6-dimethoxybenzoyl)-2ξ,3ξ-epoxy-3ξ-methoxycarbonyl-7-oxabicyclo<2.2.1>heptane

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Technology Process of 2ξ-(2,6-dimethoxybenzoyl)-2ξ,3ξ-epoxy-3ξ-methoxycarbonyl-7-oxabicyclo<2.2.1>heptane

There total 11 articles about 2ξ-(2,6-dimethoxybenzoyl)-2ξ,3ξ-epoxy-3ξ-methoxycarbonyl-7-oxabicyclo<2.2.1>heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61227-33-6
2-(2,6-dimethoxybenzoyl)-3-methoxycarbonyl-7-oxabicyclo<2.2.1>hept-2-ene

: 76505-13-0
2ξ-(2,6-dimethoxybenzoyl)-2ξ,3ξ-epoxy-3ξ-methoxycarbonyl-7-oxabicyclo<2.2.1>heptane

Guidance literature:: With dihydrogen peroxide; potassium carbonate; In water; acetone; at 0 ℃;

Reference yield:

: 2785-97-9
(2,6-dimethoxyphenyl)lithium

: 76505-13-0
2ξ-(2,6-dimethoxybenzoyl)-2ξ,3ξ-epoxy-3ξ-methoxycarbonyl-7-oxabicyclo<2.2.1>heptane

Guidance literature:: Multi-step reaction with 6 steps

1: 1.6 g

3: 0.2 g / toluene-p-sulphonic acid / benzene / 72 h / Heating

4: 70 percent / bromine / acetic acid / 0.5 h

5: lithium carbonate / dimethylformamide

6: 2 g / 30percent hydrogen peroxide, potassium carbonate / acetone; H₂O / 0 °C

With dihydrogen peroxide; bromine; lithium carbonate; potassium carbonate; toluene-4-sulfonic acid; In water; acetic acid; N,N-dimethyl-formamide; acetone; benzene;

Reference yield:

: 76504-82-0,76504-83-1
2α-(2,6-dimethoxybenzoyl)-7-oxabicyclo<2.2.1>heptane-3α-carboxylic acid

: 76505-13-0
2ξ-(2,6-dimethoxybenzoyl)-2ξ,3ξ-epoxy-3ξ-methoxycarbonyl-7-oxabicyclo<2.2.1>heptane

Guidance literature:: Multi-step reaction with 5 steps

2: 0.2 g / toluene-p-sulphonic acid / benzene / 72 h / Heating

3: 70 percent / bromine / acetic acid / 0.5 h

4: lithium carbonate / dimethylformamide

5: 2 g / 30percent hydrogen peroxide, potassium carbonate / acetone; H₂O / 0 °C

With dihydrogen peroxide; bromine; lithium carbonate; potassium carbonate; toluene-4-sulfonic acid; In water; acetic acid; N,N-dimethyl-formamide; acetone; benzene;