2-methylphenyl 2-naphthyl sulfide

Base Information

• Chemical Name: 2-methylphenyl 2-naphthyl sulfide
• CAS No.: 127567-53-7
• Molecular Formula: C₁₇H₁₄S
• Molecular Weight: 250.364
• Mol file: 127567-53-7.mol

Synonyms:2-methylphenyl 2-naphthyl sulfide

Chemical Property of 2-methylphenyl 2-naphthyl sulfide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2-methylphenyl 2-naphthyl sulfide

There total 9 articles about 2-methylphenyl 2-naphthyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

bis(2-methylphenyl)disulfide (4032-80-8) + naphthalene-2-carboxylate (93-09-4) → 2-methylphenyl 2-naphthyl sulfide (127567-53-7)

Guidance literature:

With manganese; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); 1,3-bis-(diphenylphosphino)propane; 2,2-dimethylpropanoic anhydride; zinc; In toluene; at 160 ℃; for 24h; Sealed tube; Inert atmosphere;

DOI:10.1002/ejoc.202100115

Reference yield: 91.0%

ortho-methylphenyl iodide (615-37-2) + 2-Naphthalenethiol (91-60-1) → 2-methylphenyl 2-naphthyl sulfide (127567-53-7)

Guidance literature:

With trans-9,10-dihydro-9,10-ethanoanthracene-11,12-dimethanol; caesium carbonate; copper(I) bromide; In acetonitrile; at 82 ℃; for 15h; Inert atmosphere; Sealed tube;

DOI:10.1055/s-0029-1217056

Reference yield: 89.0%

2-Naphthalenethiol (91-60-1) + 2-methylbenzoic anhydride (607-86-3) → 2-methylphenyl 2-naphthyl sulfide (127567-53-7)

Guidance literature:

With manganese; 1,3-bis-(diphenylphosphino)propane; sodium carbonate; nickel dichloride; In toluene; at 150 ℃; for 24h; Sealed tube; Inert atmosphere;

DOI:10.1021/acs.joc.9b01746

upstream raw materials:

2-methylphenyl bromide

β-naphthol

2-thiocresol

ortho-methylphenyl iodide