(R)-3-((S)-1-(3-chlorophenyl)-1,5-dimethoxypentyl)-piperidine HCl salt

Base Information

Chemical Name:(R)-3-((S)-1-(3-chlorophenyl)-1,5-dimethoxypentyl)-piperidine HCl salt
CAS No.:884512-71-4
Molecular Formula:C₁₈H₂₈ClNO₂*ClH
Molecular Weight:362.34
Hs Code.:

Synonyms:(R)-3-((S)-1-(3-chlorophenyl)-1,5-dimethoxypentyl)-piperidine HCl salt

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Chemical Property of (R)-3-((S)-1-(3-chlorophenyl)-1,5-dimethoxypentyl)-piperidine HCl salt

Chemical Property:

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Technology Process of (R)-3-((S)-1-(3-chlorophenyl)-1,5-dimethoxypentyl)-piperidine HCl salt

There total 5 articles about (R)-3-((S)-1-(3-chlorophenyl)-1,5-dimethoxypentyl)-piperidine HCl salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (R)-tert-butyl 3-((S)-1-(3-chlorophenyl)-1,5-dimethoxypentyl)piperidine-1-carboxylate

: 884512-71-4
(R)-3-((S)-1-(3-chlorophenyl)-1,5-dimethoxypentyl)-piperidine HCl salt

Guidance literature:: With hydrogenchloride; In water; acetonitrile; at 20 ℃; for 2h;

Reference yield:

: 884510-86-5
(R)-tert-butyl 3-(methoxy(methyl)carbamoyl)piperidine-1-carboxylate

: 884512-71-4
(R)-3-((S)-1-(3-chlorophenyl)-1,5-dimethoxypentyl)-piperidine HCl salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 2 h / 20 °C

2.1: iodine; magnesium / tetrahydrofuran / 1 h / Heating / reflux

2.2: 2 h / -78 - 20 °C

3.1: sodium hydride / tetrahydrofuran / 16 h / 70 °C

4.1: hydrogenchloride / water; acetonitrile / 2 h / 20 °C

With hydrogenchloride; n-butyllithium; iodine; sodium hydride; magnesium; In tetrahydrofuran; hexane; water; acetonitrile;

Reference yield:

: 884512-54-3
(R)-tert-butyl 3-((S)-1-(3-chlorophenyl)-1-hydroxy-5-methoxypentyl)piperidine-1-carboxylate

: 884512-71-4
(R)-3-((S)-1-(3-chlorophenyl)-1,5-dimethoxypentyl)-piperidine HCl salt

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran / 16 h / 70 °C

2: hydrogenchloride / water; acetonitrile / 2 h / 20 °C

With hydrogenchloride; sodium hydride; In tetrahydrofuran; water; acetonitrile;