(1R,2R,3R)-3-(3-(benzyloxy)benzyl)-2-((3S,1E)-3-hydroxyoct-1-enyl)-4-methylenecyclopentanol

Base Information

Chemical Name:(1R,2R,3R)-3-(3-(benzyloxy)benzyl)-2-((3S,1E)-3-hydroxyoct-1-enyl)-4-methylenecyclopentanol
CAS No.:1425937-43-4
Molecular Formula:C₂₈H₃₆O₃
Molecular Weight:420.592
Hs Code.:

Synonyms:(1R,2R,3R)-3-(3-(benzyloxy)benzyl)-2-((3S,1E)-3-hydroxyoct-1-enyl)-4-methylenecyclopentanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R,3R)-3-(3-(benzyloxy)benzyl)-2-((3S,1E)-3-hydroxyoct-1-enyl)-4-methylenecyclopentanol

Chemical Property:

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Technology Process of (1R,2R,3R)-3-(3-(benzyloxy)benzyl)-2-((3S,1E)-3-hydroxyoct-1-enyl)-4-methylenecyclopentanol

There total 5 articles about (1R,2R,3R)-3-(3-(benzyloxy)benzyl)-2-((3S,1E)-3-hydroxyoct-1-enyl)-4-methylenecyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₀H₆₄O₃Si₂

: 1425937-43-4
(1R,2R,3R)-3-(3-(benzyloxy)benzyl)-2-((3S,1E)-3-hydroxyoct-1-enyl)-4-methylenecyclopentanol

Guidance literature:: With toluene-4-sulfonic acid; In water; acetone; at 25 ℃; for 1h;

Reference yield:

: 1425937-39-8
(2R,3R,4R)-2-(3-(benzyloxy)benzyl)-4-triethylsilyloxy-3-((3S,1E)-3-triethylsilyloxyoct-1-enyl)cyclopentanone

: 74-95-3
1,1-dibromomethane

: 1425937-43-4
(1R,2R,3R)-3-(3-(benzyloxy)benzyl)-2-((3S,1E)-3-hydroxyoct-1-enyl)-4-methylenecyclopentanol

Guidance literature:: (2R,3R,4R)-2-(3-(benzyloxy)benzyl)-4-triethylsilyloxy-3-((3S,1E)-3-triethylsilyloxyoct-1-enyl)cyclopentanone; 1,1-dibromomethane; With toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; at 25 ℃; for 1.5h; Cooling with ice;

With toluene-4-sulfonic acid; In water; acetone; at 20 ℃; for 1h;

Reference yield:

: 1425937-59-2
(3R)-1-[3-(benzyloxy)benzyl]-5-oxo-3-(triethylsilyloxy)cyclopent-1-ene

: 1425937-43-4
(1R,2R,3R)-3-(3-(benzyloxy)benzyl)-2-((3S,1E)-3-hydroxyoct-1-enyl)-4-methylenecyclopentanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; copper(l) cyanide; methyllithium / diethyl ether; hexane; tetrahydrofuran / 0.5 h / -70 °C

1.2: 0.5 h / -70 °C

2.1: toluene-4-sulfonic acid / tetrahydrofuran; dichloromethane / 1.5 h / 25 °C / Cooling with ice

2.2: 1 h / 20 °C

With n-butyllithium; methyllithium; copper(l) cyanide; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; hexane; dichloromethane;