methyl 2-benzyl-4,6-dioxoheptanoate

Base Information

Chemical Name:methyl 2-benzyl-4,6-dioxoheptanoate
CAS No.:103437-82-7
Molecular Formula:C₁₅H₁₈O₄
Molecular Weight:262.306
Hs Code.:

Synonyms:methyl 2-benzyl-4,6-dioxoheptanoate

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Chemical Property of methyl 2-benzyl-4,6-dioxoheptanoate

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Technology Process of methyl 2-benzyl-4,6-dioxoheptanoate

There total 6 articles about methyl 2-benzyl-4,6-dioxoheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96017-60-6
2-benzyl-4-pentynoic acid

: 103437-82-7
methyl 2-benzyl-4,6-dioxoheptanoate

Guidance literature:: Multi-step reaction with 6 steps

1: 72.4 percent / N-iodosuccinimide, NaHCO₃, tetrabutylammonium hydroxide / CH₂Cl₂; H₂O / 0.5 h

2: 0.43 g / iodine / CH₂Cl₂ / 90 h / Ambient temperature; in the dark

3: PdCl₂(Ph₃P)2, CuI, Et₃N

4: 31 percent / AgNO₃, KCN / ethanol; H₂O / 0.5 h / 0 °C / in the dark

5: 1 M NaOH / H₂O / 5 h / Ambient temperature

6: diethyl ether

With potassium cyanide; bis-triphenylphosphine-palladium(II) chloride; sodium hydroxide; N-iodo-succinimide; copper(l) iodide; tetra(n-butyl)ammonium hydroxide; iodine; sodium hydrogencarbonate; silver nitrate; triethylamine; In diethyl ether; ethanol; dichloromethane; water;
DOI:10.1021/ja00278a038

Reference yield:

: 93040-53-0
3-benzyl-5(E)-(iodomethylene)tetrahydro-2-furanone

: 103437-82-7
methyl 2-benzyl-4,6-dioxoheptanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 0.43 g / iodine / CH₂Cl₂ / 90 h / Ambient temperature; in the dark

2: PdCl₂(Ph₃P)2, CuI, Et₃N

3: 31 percent / AgNO₃, KCN / ethanol; H₂O / 0.5 h / 0 °C / in the dark

4: 1 M NaOH / H₂O / 5 h / Ambient temperature

5: diethyl ether

With potassium cyanide; bis-triphenylphosphine-palladium(II) chloride; sodium hydroxide; copper(l) iodide; iodine; silver nitrate; triethylamine; In diethyl ether; ethanol; dichloromethane; water;
DOI:10.1021/ja00278a038

Reference yield:

: 103437-61-2
3-benzyl-5(Z)-(iodomethylene)tetrahydro-2-furanone

: 103437-82-7
methyl 2-benzyl-4,6-dioxoheptanoate

Guidance literature:: Multi-step reaction with 4 steps

1: PdCl₂(Ph₃P)2, CuI, Et₃N

2: 31 percent / AgNO₃, KCN / ethanol; H₂O / 0.5 h / 0 °C / in the dark

3: 1 M NaOH / H₂O / 5 h / Ambient temperature

4: diethyl ether

With potassium cyanide; bis-triphenylphosphine-palladium(II) chloride; sodium hydroxide; copper(l) iodide; silver nitrate; triethylamine; In diethyl ether; ethanol; water;
DOI:10.1021/ja00278a038