(S)-2-tert-Butoxycarbonylamino-5-(10-methoxy-anthracen-9-yl)-pentanoic acid benzyl ester

Base Information

Chemical Name:(S)-2-tert-Butoxycarbonylamino-5-(10-methoxy-anthracen-9-yl)-pentanoic acid benzyl ester
CAS No.:198275-38-6
Molecular Formula:C₃₂H₃₅NO₅
Molecular Weight:513.634
Hs Code.:

Synonyms:(S)-2-tert-Butoxycarbonylamino-5-(10-methoxy-anthracen-9-yl)-pentanoic acid benzyl ester

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Chemical Property of (S)-2-tert-Butoxycarbonylamino-5-(10-methoxy-anthracen-9-yl)-pentanoic acid benzyl ester

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Technology Process of (S)-2-tert-Butoxycarbonylamino-5-(10-methoxy-anthracen-9-yl)-pentanoic acid benzyl ester

There total 11 articles about (S)-2-tert-Butoxycarbonylamino-5-(10-methoxy-anthracen-9-yl)-pentanoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 198275-38-6
(S)-2-tert-Butoxycarbonylamino-5-(10-methoxy-anthracen-9-yl)-pentanoic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / dioxane; H₂O

2: Et₃N / dimethylformamide

With triethylamine; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1055/s-1997-5792

Reference yield:

: 198275-32-0
9-But-3-enyl-10-methoxy-anthracene

: 198275-38-6
(S)-2-tert-Butoxycarbonylamino-5-(10-methoxy-anthracen-9-yl)-pentanoic acid benzyl ester

Guidance literature:: Multi-step reaction with 10 steps

1: 73 percent / OsO₄, NMO / 2-methyl-propan-2-ol; tetrahydrofuran; H₂O

2: 90 percent / NaIO₄ / acetone; H₂O

3: NaBH₄ / methanol / 0 °C

4: 79 percent / CBr₄, PPh₃ / toluene

5: 72 percent / NaH / dimethylformamide / 0 deg C up to RT

6: 95 percent / 3M NaOH / methanol

7: 70 percent / CSA / tetrahydrofuran / Heating

8: Aspergillus genus acylase, CoCl₂ / dimethylsulfoxide; H₂O / 35 - 40 °C / pH 7.0-7.2

9: Et₃N / dioxane; H₂O

10: Et₃N / dimethylformamide

With sodium hydroxide; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; carbon tetrabromide; Aspergillus genus acylase; camphor-10-sulfonic acid; sodium hydride; triethylamine; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol;
DOI:10.1055/s-1997-5792

Reference yield:

: 198275-49-9
3-(10-Methoxy-anthracen-9-yl)-propionaldehyde

: 198275-38-6
(S)-2-tert-Butoxycarbonylamino-5-(10-methoxy-anthracen-9-yl)-pentanoic acid benzyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: NaBH₄ / methanol / 0 °C

2: 79 percent / CBr₄, PPh₃ / toluene

3: 72 percent / NaH / dimethylformamide / 0 deg C up to RT

4: 95 percent / 3M NaOH / methanol

5: 70 percent / CSA / tetrahydrofuran / Heating

6: Aspergillus genus acylase, CoCl₂ / dimethylsulfoxide; H₂O / 35 - 40 °C / pH 7.0-7.2

7: Et₃N / dioxane; H₂O

8: Et₃N / dimethylformamide

With sodium hydroxide; sodium tetrahydroborate; carbon tetrabromide; Aspergillus genus acylase; camphor-10-sulfonic acid; sodium hydride; triethylamine; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1055/s-1997-5792