(S)-1,1-dimethylethyl 4-[1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]benzoate

Base Information

Chemical Name:(S)-1,1-dimethylethyl 4-[1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]benzoate
CAS No.:367258-69-3
Molecular Formula:C₁₈H₂₇NO₅
Molecular Weight:337.416
Hs Code.:

Synonyms:(S)-1,1-dimethylethyl 4-[1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1,1-dimethylethyl 4-[1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]benzoate

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Technology Process of (S)-1,1-dimethylethyl 4-[1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]benzoate

There total 2 articles about (S)-1,1-dimethylethyl 4-[1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 4248-19-5
tert-butyl carbazate

: 84740-98-7
4-t-butyloxycarbonylstyrene

: 367258-69-3
(S)-1,1-dimethylethyl 4-[1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]benzoate

Guidance literature:: tert-butyl carbazate; With sodium hydroxide; tert-butylhypochlorite; In propan-1-ol; water; at 20 ℃; for 0.333333h;

4-t-butyloxycarbonylstyrene; With potassium osmate(VI); Hydroquinone 1,4-phthalazinediyl diether; In propan-1-ol; water; at 0 ℃; for 12h; Further stages.;
DOI:10.1021/jo010512b

Reference yield:

: 1075-49-6
4-ethenylbenzoic acid

: 367258-69-3
(S)-1,1-dimethylethyl 4-[1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 66 percent / benzene / 4 h / Heating

2.1: tert-butyl hypochlorite; NaOH / propan-1-ol; H₂O / 0.33 h / 20 °C

2.2: 70 percent / (DHQ)2Phal; K₂OsO₄*2H₂O / propan-1-ol; H₂O / 12 h / 0 °C

With sodium hydroxide; tert-butylhypochlorite; In propan-1-ol; water; benzene;
DOI:10.1021/jo010512b