1,1-dimethylethyl 4-[(1S)-1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]cyclohexaneacetate

Base Information

Chemical Name:1,1-dimethylethyl 4-[(1S)-1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]cyclohexaneacetate
CAS No.:367258-70-6
Molecular Formula:C₁₈H₃₃NO₅
Molecular Weight:343.464
Hs Code.:

Synonyms:1,1-dimethylethyl 4-[(1S)-1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]cyclohexaneacetate

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Chemical Property of 1,1-dimethylethyl 4-[(1S)-1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]cyclohexaneacetate

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Technology Process of 1,1-dimethylethyl 4-[(1S)-1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]cyclohexaneacetate

There total 3 articles about 1,1-dimethylethyl 4-[(1S)-1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]cyclohexaneacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 367258-69-3
(S)-1,1-dimethylethyl 4-[1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]benzoate

: 367258-70-6
1,1-dimethylethyl 4-[(1S)-1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]cyclohexaneacetate

Guidance literature:: With hydrogen; 10percent Rh/C; In methanol; for 72h; under 3102.97 Torr;
DOI:10.1021/jo010512b

Reference yield:

: 1075-49-6
4-ethenylbenzoic acid

: 367258-70-6
1,1-dimethylethyl 4-[(1S)-1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]cyclohexaneacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 66 percent / benzene / 4 h / Heating

2.1: tert-butyl hypochlorite; NaOH / propan-1-ol; H₂O / 0.33 h / 20 °C

2.2: 70 percent / (DHQ)2Phal; K₂OsO₄*2H₂O / propan-1-ol; H₂O / 12 h / 0 °C

3.1: 83 percent / H₂ / 10percent Rh/C / methanol / 72 h / 3102.97 Torr

With sodium hydroxide; tert-butylhypochlorite; hydrogen; 10percent Rh/C; In methanol; propan-1-ol; water; benzene;
DOI:10.1021/jo010512b

Reference yield:

: 84740-98-7
4-t-butyloxycarbonylstyrene

: 367258-70-6
1,1-dimethylethyl 4-[(1S)-1-[[(1,1-dimethylethoxy)carbonyl]amino]-2-hydroxyethyl]cyclohexaneacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert-butyl hypochlorite; NaOH / propan-1-ol; H₂O / 0.33 h / 20 °C

1.2: 70 percent / (DHQ)2Phal; K₂OsO₄*2H₂O / propan-1-ol; H₂O / 12 h / 0 °C

2.1: 83 percent / H₂ / 10percent Rh/C / methanol / 72 h / 3102.97 Torr

With sodium hydroxide; tert-butylhypochlorite; hydrogen; 10percent Rh/C; In methanol; propan-1-ol; water;
DOI:10.1021/jo010512b