C₄₁H₆₄O₉Si₂

Base Information

Chemical Name:C₄₁H₆₄O₉Si₂
CAS No.:285118-36-7
Molecular Formula:C₄₁H₆₄O₉Si₂
Molecular Weight:757.125
Hs Code.:

C<sub>41</sub>H<sub>64</sub>O<sub>9</sub>Si<sub>2</sub>

Synonyms:C₄₁H₆₄O₉Si₂

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Chemical Property of C₄₁H₆₄O₉Si₂

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Technology Process of C₄₁H₆₄O₉Si₂

There total 11 articles about C₄₁H₆₄O₉Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 285118-35-6
C₄₁H₆₂O₉Si₂

: 285118-36-7
C₄₁H₆₄O₉Si₂

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; ethanol; at 20 ℃;
DOI:10.1016/S0040-4039(00)00379-8

Reference yield:

: 994-30-9
triethylsilyl chloride

: 285118-36-7
C₄₁H₆₄O₉Si₂

Guidance literature:: Multi-step reaction with 10 steps

1: 69 percent / imidazole / dimethylformamide / 20 °C

2: 59 percent / Red-Al / tetrahydrofuran / 0 °C

3: 93 percent / pyridine / CH₂Cl₂ / -15 °C

4: 63 percent / Et₄NBr; BF₃*Et₂O / CH₂Cl₂ / 20 °C

5: 72 percent / PBu₃; DEAD / dimethylformamide / 20 °C

6: 53 percent / n-Bu₄NI; BF₃*Et₂O / CH₂Cl₂ / 20 °C

7: 70 percent / Zn / tetrahydrofuran / Heating

8: 83 percent / DMAP / CH₂Cl₂ / 20 °C

9: 59 percent / tetrahydrofuran / -72 °C

10: 49 percent / NaBH₄ / ethanol; tetrahydrofuran / 20 °C

With pyridine; 1H-imidazole; dmap; sodium tetrahydroborate; tributylphosphine; boron trifluoride diethyl etherate; tetraethylammonium bromide; tetra-(n-butyl)ammonium iodide; sodium bis(2-methoxyethoxy)aluminium dihydride; zinc; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; 1: Etherification / 2: Hydrolysis / 3: Esterification / 4: Ring cleavage / 5: Epoxidation / 6: Ring cleavage / 7: Cyclization / 8: Acetylation / 9: Ring cleavage / 10: Reduction;
DOI:10.1016/S0040-4039(00)00379-8

Reference yield:

: 92950-42-0
13-dehydro-10-deacetylbaccatin III

: 285118-36-7
C₄₁H₆₄O₉Si₂

Guidance literature:: Multi-step reaction with 10 steps

1: 69 percent / imidazole / dimethylformamide / 20 °C

2: 59 percent / Red-Al / tetrahydrofuran / 0 °C

3: 93 percent / pyridine / CH₂Cl₂ / -15 °C

4: 63 percent / Et₄NBr; BF₃*Et₂O / CH₂Cl₂ / 20 °C

5: 72 percent / PBu₃; DEAD / dimethylformamide / 20 °C

6: 53 percent / n-Bu₄NI; BF₃*Et₂O / CH₂Cl₂ / 20 °C

7: 70 percent / Zn / tetrahydrofuran / Heating

8: 83 percent / DMAP / CH₂Cl₂ / 20 °C

9: 59 percent / tetrahydrofuran / -72 °C

10: 49 percent / NaBH₄ / ethanol; tetrahydrofuran / 20 °C

With pyridine; 1H-imidazole; dmap; sodium tetrahydroborate; tributylphosphine; boron trifluoride diethyl etherate; tetraethylammonium bromide; tetra-(n-butyl)ammonium iodide; sodium bis(2-methoxyethoxy)aluminium dihydride; zinc; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; 1: Etherification / 2: Hydrolysis / 3: Esterification / 4: Ring cleavage / 5: Epoxidation / 6: Ring cleavage / 7: Cyclization / 8: Acetylation / 9: Ring cleavage / 10: Reduction;
DOI:10.1016/S0040-4039(00)00379-8