N-[1-(dimethylphenylsilyl)propyl]-N-methyl-N'-(4-methylphenyl)sulfonylglycinamide

Base Information

Chemical Name:N-[1-(dimethylphenylsilyl)propyl]-N-methyl-N'-(4-methylphenyl)sulfonylglycinamide
CAS No.:449774-94-1
Molecular Formula:C₂₁H₃₀N₂O₃SSi
Molecular Weight:418.632
Hs Code.:

Synonyms:N-[1-(dimethylphenylsilyl)propyl]-N-methyl-N'-(4-methylphenyl)sulfonylglycinamide

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Chemical Property of N-[1-(dimethylphenylsilyl)propyl]-N-methyl-N'-(4-methylphenyl)sulfonylglycinamide

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Technology Process of N-[1-(dimethylphenylsilyl)propyl]-N-methyl-N'-(4-methylphenyl)sulfonylglycinamide

There total 2 articles about N-[1-(dimethylphenylsilyl)propyl]-N-methyl-N'-(4-methylphenyl)sulfonylglycinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 70-55-3
toluene-4-sulfonamide

: 449774-99-6
N-[1-(dimethylphenylsilyl)propyl]-N-methylchloroacetamide

: 449774-94-1
N-[1-(dimethylphenylsilyl)propyl]-N-methyl-N'-(4-methylphenyl)sulfonylglycinamide

Guidance literature:: toluene-4-sulfonamide; With sodium hydride; In N,N-dimethyl-formamide; at 60 ℃; for 2h;

N-[1-(dimethylphenylsilyl)propyl]-N-methylchloroacetamide; In N,N-dimethyl-formamide; at 60 ℃; for 2h; Further stages.;
DOI:10.1039/b111106j

Reference yield:

: N-methyl-1-(dimethylphenylsilyl)propylamine

: 449774-94-1
N-[1-(dimethylphenylsilyl)propyl]-N-methyl-N'-(4-methylphenyl)sulfonylglycinamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 60 percent / TEA / CH₂Cl₂ / 20 °C

2.1: NaH / dimethylformamide / 2 h / 60 °C

2.2: 61 percent / dimethylformamide / 2 h / 60 °C

With TEA; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b111106j

Reference yield: 48.0%

: 449774-94-1
N-[1-(dimethylphenylsilyl)propyl]-N-methyl-N'-(4-methylphenyl)sulfonylglycinamide

: 1,4-diaza-1-methyl-2-ethyl-3-(4-methylphenylsulfonyl)cyclopent-5-one

Guidance literature:: With 2,2,2-trifluoroethanol; N,N,N,N-tetraethylammonium tetrafluoroborate; In dichloromethane; at 20 ℃; Electrochemical reaction;
DOI:10.1039/b111106j