benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteine phenylhydrazide

Base Information

Chemical Name:benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteine phenylhydrazide
CAS No.:104903-57-3
Molecular Formula:C₅₈H₇₀N₁₀O₁₁S₂
Molecular Weight:1147.39
Hs Code.:

Synonyms:benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteine phenylhydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteine phenylhydrazide

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Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteine phenylhydrazide

There total 3 articles about benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteine phenylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 39621-64-2
S-benzyl-N-[(benzyloxy)carbonyl]cysteinyltyrosine

: 104903-65-3
isoleucyl-glutaminyl-asparaginyl-S-benzylcysteine phenylhydrazide trifluoroacetate

: 104903-57-3
benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteine phenylhydrazide

Guidance literature:: With thermolysin; In water; N,N-dimethyl-formamide; at 38 ℃; for 24h; pH 7, CaCl₂;
DOI:10.1135/cccc19852775

Reference yield:

: 3257-18-9
benzyloxycarbonyl-S-benzylcysteine

: 104903-57-3
benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteine phenylhydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / papain / dimethylformamide; H₂O / 24 h / 38 °C / ethylenediaminetetraacetic acid, cysteine hydrochloride, pH 4.8

2: 75 percent / FeCl₃ / H₂O; dioxane / 0.5 h / 35 °C

3: 72 percent / thermolysin / dimethylformamide; H₂O / 24 h / 38 °C / pH 7, CaCl₂

With iron(III) chloride; papain; thermolysin; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1135/cccc19852775

Reference yield:

: 104903-60-8
benzyloxycarbonyl-S-benzylcysteinyl-tyrosine phenylhydrazide

: 104903-57-3
benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteine phenylhydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / FeCl₃ / H₂O; dioxane / 0.5 h / 35 °C

2: 72 percent / thermolysin / dimethylformamide; H₂O / 24 h / 38 °C / pH 7, CaCl₂

With iron(III) chloride; thermolysin; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1135/cccc19852775