N-benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparginyl-S-benzylcysteine

Base Information

Chemical Name:N-benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparginyl-S-benzylcysteine
CAS No.:27493-87-4
Molecular Formula:C₅₂H₆₄N₈O₁₂S₂
Molecular Weight:1057.26
Hs Code.:

Synonyms:N-benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparginyl-S-benzylcysteine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparginyl-S-benzylcysteine

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Technology Process of N-benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparginyl-S-benzylcysteine

There total 6 articles about N-benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparginyl-S-benzylcysteine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 104903-57-3
benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteine phenylhydrazide

: 27493-87-4
N-benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparginyl-S-benzylcysteine

Guidance literature:: With iron(III) chloride; In water; N,N-dimethyl-formamide; at 35 ℃; for 0.5h;
DOI:10.1135/cccc19852775

Reference yield:

: 3257-18-9
benzyloxycarbonyl-S-benzylcysteine

: 27493-87-4
N-benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparginyl-S-benzylcysteine

Guidance literature:: Multi-step reaction with 4 steps

1: 52 percent / papain / dimethylformamide; H₂O / 24 h / 38 °C / ethylenediaminetetraacetic acid, cysteine hydrochloride, pH 4.8

2: 75 percent / FeCl₃ / H₂O; dioxane / 0.5 h / 35 °C

3: 72 percent / thermolysin / dimethylformamide; H₂O / 24 h / 38 °C / pH 7, CaCl₂

4: 51 percent / FeCl₃ / H₂O; dimethylformamide / 0.5 h / 35 °C

With iron(III) chloride; papain; thermolysin; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1135/cccc19852775

Reference yield:

: 39621-64-2
S-benzyl-N-[(benzyloxy)carbonyl]cysteinyltyrosine

: 27493-87-4
N-benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparginyl-S-benzylcysteine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / thermolysin / dimethylformamide; H₂O / 24 h / 38 °C / pH 7, CaCl₂

2: 51 percent / FeCl₃ / H₂O; dimethylformamide / 0.5 h / 35 °C

With iron(III) chloride; thermolysin; In water; N,N-dimethyl-formamide;
DOI:10.1135/cccc19852775