2-Imino-5-((phenylamino)methyl)-3-((phenyl(phenylazo)methylene)amino)-4-thiazolidinone

Base Information

• Chemical Name: 2-Imino-5-((phenylamino)methyl)-3-((phenyl(phenylazo)methylene)amino)-4-thiazolidinone
• CAS No.: 152449-61-1
• Molecular Formula: C₂₃H₂₀N₆OS
• Molecular Weight: 428.517
• Mol file: 152449-61-1.mol

Synonyms:2-Imino-5-((phenylamino)methyl)-3-((phenyl(phenylazo)methylene)amino)-4-thiazolidinone;4-Thiazolidinone, 2-imino-5-((phenylamino)methyl)-3-((phenyl(phenylazo)methylene)amino)-;152449-61-1;LS-151790

Chemical Property of 2-Imino-5-((phenylamino)methyl)-3-((phenyl(phenylazo)methylene)amino)-4-thiazolidinone

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 591.314°C at 760 mmHg
• Flash Point: 311.415°C
• Density: 1.312g/cm³
• XLogP3: 5.9
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 7
• Exact Mass: 428.14193046
• Heavy Atom Count: 31
• Complexity: 678

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=NN2C(=O)C(SC2=N)CNC3=CC=CC=C3)N=NC4=CC=CC=C4
• Isomeric SMILES: C1=CC=C(C=C1)/C(=N/N2C(=O)C(SC2=N)CNC3=CC=CC=C3)/N=NC4=CC=CC=C4

Technology Process of 2-Imino-5-((phenylamino)methyl)-3-((phenyl(phenylazo)methylene)amino)-4-thiazolidinone

There total 4 articles about 2-Imino-5-((phenylamino)methyl)-3-((phenyl(phenylazo)methylene)amino)-4-thiazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(Benzylideneamino)-2-imino-4-thiazolidinone → C23H20N6OS (152449-61-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) NaNO₂, gl. AcOH, aq. HCl, 2) pyridine / 1) water, 0-5 deg C, 2) 4 h, r.t.

2: dioxane; H₂O / 6 h / Heating

With pyridine; hydrogenchloride; acetic acid; sodium nitrite; In 1,4-dioxane; water;

Reference yield:

1-benzylidene thiosemicarbazide (1627-73-2) → C23H20N6OS (152449-61-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 70 percent / NaOAc, AcOH / 8 h / Heating

2: 1) NaNO₂, gl. AcOH, aq. HCl, 2) pyridine / 1) water, 0-5 deg C, 2) 4 h, r.t.

3: dioxane; H₂O / 6 h / Heating

With pyridine; hydrogenchloride; sodium acetate; acetic acid; sodium nitrite; In 1,4-dioxane; water;

Reference yield:

aniline (62-53-3) → C23H20N6OS (152449-61-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) NaNO₂, gl. AcOH, aq. HCl, 2) pyridine / 1) water, 0-5 deg C, 2) 4 h, r.t.

2: dioxane; H₂O / 6 h / Heating

With pyridine; hydrogenchloride; acetic acid; sodium nitrite; In 1,4-dioxane; water;

upstream raw materials:

formaldehyd

aniline

C₁₆H₁₃N₅OS

1-benzylidene thiosemicarbazide