N-methoxy-carbonyl-N-((2E,6Z)-8-acetoxy-2,6-dimethyl-octa-2,6-dienyl)-p-toluenesulfonamide

Base Information

Chemical Name:N-methoxy-carbonyl-N-((2E,6Z)-8-acetoxy-2,6-dimethyl-octa-2,6-dienyl)-p-toluenesulfonamide
CAS No.:600153-10-4
Molecular Formula:C₂₁H₂₉NO₆S
Molecular Weight:423.53
Hs Code.:

Synonyms:N-methoxy-carbonyl-N-((2E,6Z)-8-acetoxy-2,6-dimethyl-octa-2,6-dienyl)-p-toluenesulfonamide

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Chemical Property of N-methoxy-carbonyl-N-((2E,6Z)-8-acetoxy-2,6-dimethyl-octa-2,6-dienyl)-p-toluenesulfonamide

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Technology Process of N-methoxy-carbonyl-N-((2E,6Z)-8-acetoxy-2,6-dimethyl-octa-2,6-dienyl)-p-toluenesulfonamide

There total 3 articles about N-methoxy-carbonyl-N-((2E,6Z)-8-acetoxy-2,6-dimethyl-octa-2,6-dienyl)-p-toluenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 70238-37-8
(2'Z,6'E)-Essigsaeure-(8'-hydroxy-3',7'-dimethyl-2',6'-octadien-1'-yl)ester

: 14437-03-7
methyl tosylcarbamate

: 600153-10-4
N-methoxy-carbonyl-N-((2E,6Z)-8-acetoxy-2,6-dimethyl-octa-2,6-dienyl)-p-toluenesulfonamide

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; at 20 ℃; for 2.7h;
DOI:10.1021/ol053141k

Reference yield:

: 141-12-8,8022-83-1
neryl acetate

: 600153-10-4
N-methoxy-carbonyl-N-((2E,6Z)-8-acetoxy-2,6-dimethyl-octa-2,6-dienyl)-p-toluenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / selenium(IV) oxide; tert-butyl hydroperoxide; salicylic acid / CH₂Cl₂ / 23 h / 20 °C

2: 97 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran; toluene / 2.7 h / 20 °C

With tert.-butylhydroperoxide; selenium(IV) oxide; triphenylphosphine; salicylic acid; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; toluene; 2: Mitsunobu reaction;
DOI:10.1021/ol053141k

Reference yield:

: 4083-64-1
Tosyl isocyanate

: 600153-10-4
N-methoxy-carbonyl-N-((2E,6Z)-8-acetoxy-2,6-dimethyl-octa-2,6-dienyl)-p-toluenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 0 - 20 °C

2: 97 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran; toluene / 2.7 h / 20 °C

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; 2: Mitsunobu reaction;
DOI:10.1021/ol053141k