((((CH₃)2CH)2C₆H₃NCCH₃)2PdCHCH₂CH₃C(O)OCH₃)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(C₂₈H₄₀N₂)PdCHCH₂CH₃C(O)OCH₃][B(C₆H₃(CF₃)2)4]

Base Information

• Chemical Name: ((((CH₃)2CH)2C₆H₃NCCH₃)2PdCHCH₂CH₃C(O)OCH₃)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(C₂₈H₄₀N₂)PdCHCH₂CH₃C(O)OCH₃][B(C₆H₃(CF₃)2)4]
• CAS No.: 201007-41-2
• Molecular Formula: C₃₂H₁₂BF₂₄*C₃₃H₄₉N₂O₂Pd
• Molecular Weight: 1475.4

Synonyms:((((CH₃)2CH)2C₆H₃NCCH₃)2PdCHCH₂CH₃C(O)OCH₃)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(C₂₈H₄₀N₂)PdCHCH₂CH₃C(O)OCH₃][B(C₆H₃(CF₃)2)4]

Chemical Property of ((((CH₃)2CH)2C₆H₃NCCH₃)2PdCHCH₂CH₃C(O)OCH₃)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(C₂₈H₄₀N₂)PdCHCH₂CH₃C(O)OCH₃][B(C₆H₃(CF₃)2)4]

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Technology Process of ((((CH₃)2CH)2C₆H₃NCCH₃)2PdCHCH₂CH₃C(O)OCH₃)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(C₂₈H₄₀N₂)PdCHCH₂CH₃C(O)OCH₃][B(C₆H₃(CF₃)2)4]

There total 1 articles about ((((CH₃)2CH)2C₆H₃NCCH₃)2PdCHCH₂CH₃C(O)OCH₃)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(C₂₈H₄₀N₂)PdCHCH₂CH₃C(O)OCH₃][B(C₆H₃(CF₃)2)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

[(2,6-iPrC6H3NC(Me)C(Me)N-2,6-iPrC6H3)Pd(CH3)(Cl)] + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → ((((CH3)2CH)2C6H3NCCH3)2PdCHCH2CH3C(O)OCH3)(1+)*B(C6H3(CF3)2)4(1-) = [(C28H40N2)Pd(C5H9O2)][B(C8H3F6)4] (181709-52-4) + ((((CH3)2CH)2C6H3NCCH3)2PdCHCH2CH3C(O)OCH3)(1+)*B(C6H3(CF3)2)4(1-)=[(C28H40N2)PdCHCH2CH3C(O)OCH3][B(C6H3(CF3)2)4] (201007-41-2) + [(2,6-iPr2C6H3NC(Me)C(Me)NC-2,6-iPr2C6H3)Pd(CH2)3C(O)OMe](B(3,5-C6H3(CF3)2)4) (171901-49-8)

Guidance literature:

In diethyl ether; byproducts: NaCl; inert atm.; stirring (2 days), room temp.; recrystn. (CH2Cl2, -30°C), filtn (NaCl removal); products not sepd. ; elem. anal.;

DOI:10.1021/ja964144i

upstream raw materials:

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

acrylic acid methyl ester

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