(2R,3R)-4-(tert-butyldiphenylsilyloxy)-2,3-epoxybutanal dimethyl acetal

Base Information

Chemical Name:(2R,3R)-4-(tert-butyldiphenylsilyloxy)-2,3-epoxybutanal dimethyl acetal
CAS No.:157483-64-2
Molecular Formula:C₂₂H₃₀O₄Si
Molecular Weight:386.563
Hs Code.:

Synonyms:(2R,3R)-4-(tert-butyldiphenylsilyloxy)-2,3-epoxybutanal dimethyl acetal

Suppliers and Price of (2R,3R)-4-(tert-butyldiphenylsilyloxy)-2,3-epoxybutanal dimethyl acetal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2R,3R)-4-(tert-butyldiphenylsilyloxy)-2,3-epoxybutanal dimethyl acetal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2R,3R)-4-(tert-butyldiphenylsilyloxy)-2,3-epoxybutanal dimethyl acetal

There total 1 articles about (2R,3R)-4-(tert-butyldiphenylsilyloxy)-2,3-epoxybutanal dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 131484-50-9
(2R,3R)-3-(((tert-butyldiphenylsilyl)oxy)methyl)oxirane-2-carbaldehyde

: 149-73-5
trimethyl orthoformate

: 157483-64-2
(2R,3R)-4-(tert-butyldiphenylsilyloxy)-2,3-epoxybutanal dimethyl acetal

Guidance literature:: With amberlyst-15; at 0 - 4 ℃; for 2h;

Reference yield:

: 157483-64-2
(2R,3R)-4-(tert-butyldiphenylsilyloxy)-2,3-epoxybutanal dimethyl acetal

: (2R,3S)-3-Azido-4-(tert-butyl-diphenyl-silanyloxy)-2-hydroxy-butyraldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent Turnov_. / sodium azide, ammonium chloride / methanol; H₂O / 44 h / Heating

2: CF₃CO₂H / CHCl₃; H₂O / 2.5 h / 0 °C

With sodium azide; ammonium chloride; trifluoroacetic acid; In methanol; chloroform; water;