C₆₁H₆₈O₁₃

Base Information

Chemical Name:C₆₁H₆₈O₁₃
CAS No.:324740-37-6
Molecular Formula:C₆₁H₆₈O₁₃
Molecular Weight:1009.2
Hs Code.:

C<sub>61</sub>H<sub>68</sub>O<sub>13</sub>

Synonyms:C₆₁H₆₈O₁₃

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Chemical Property of C₆₁H₆₈O₁₃

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Technology Process of C₆₁H₆₈O₁₃

There total 7 articles about C₆₁H₆₈O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 324740-36-5
C₇₇H₈₆O₁₃Si

: 324740-37-6
C₆₁H₆₈O₁₃

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/S0040-4039(00)01889-X

Reference yield:

: 324740-29-6
3-O-(tert-butyldiphenylsilyl)diosgenin

: 324740-37-6
C₆₁H₆₈O₁₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: Br₂ / CHCl₃ / 0 - 20 °C

2.1: KHSO₅; NaHCO₃ / acetone; CH₂Cl₂ / 20 °C

3.1: 35 percent / acetic acid

4.1: Zn; NH₄Cl / ethanol / Heating

5.1: K₂CO₃ / tetrahydrofuran; methanol / 20 °C

5.2: TMSOTf / CH₂Cl₂ / -78 - 20 °C

6.1: 86 percent / TBAF / tetrahydrofuran / 20 °C

With potassium peroxomonosulfate; tetrabutyl ammonium fluoride; bromine; sodium hydrogencarbonate; potassium carbonate; ammonium chloride; zinc; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; acetic acid; acetone;
DOI:10.1016/S0040-4039(00)01889-X

Reference yield:

: 324740-30-9
C₄₃H₆₀Br₂O₃Si

: 324740-37-6
C₆₁H₆₈O₁₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: KHSO₅; NaHCO₃ / acetone; CH₂Cl₂ / 20 °C

2.1: 35 percent / acetic acid

3.1: Zn; NH₄Cl / ethanol / Heating

4.1: K₂CO₃ / tetrahydrofuran; methanol / 20 °C

4.2: TMSOTf / CH₂Cl₂ / -78 - 20 °C

5.1: 86 percent / TBAF / tetrahydrofuran / 20 °C

With potassium peroxomonosulfate; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; potassium carbonate; ammonium chloride; zinc; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetic acid; acetone;
DOI:10.1016/S0040-4039(00)01889-X