benzyl 27-oxo-6,9,15,18-tetraoxa-12,25-diazatetracyclo[21.3.1.0(5,26).0(19,24)]heptacosa-1⁽²⁶⁾,2,4,19,21,23-hexaene-12-carboxylate

Base Information

• Chemical Name: benzyl 27-oxo-6,9,15,18-tetraoxa-12,25-diazatetracyclo[21.3.1.0(5,26).0(19,24)]heptacosa-1⁽²⁶⁾,2,4,19,21,23-hexaene-12-carboxylate
• CAS No.: 1315451-39-8
• Molecular Formula: C₂₉H₃₀N₂O₇
• Molecular Weight: 518.566

Synonyms:benzyl 27-oxo-6,9,15,18-tetraoxa-12,25-diazatetracyclo[21.3.1.0(5,26).0(19,24)]heptacosa-1⁽²⁶⁾,2,4,19,21,23-hexaene-12-carboxylate

Chemical Property of benzyl 27-oxo-6,9,15,18-tetraoxa-12,25-diazatetracyclo[21.3.1.0(5,26).0(19,24)]heptacosa-1⁽²⁶⁾,2,4,19,21,23-hexaene-12-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl 27-oxo-6,9,15,18-tetraoxa-12,25-diazatetracyclo[21.3.1.0(5,26).0(19,24)]heptacosa-1⁽²⁶⁾,2,4,19,21,23-hexaene-12-carboxylate

There total 4 articles about benzyl 27-oxo-6,9,15,18-tetraoxa-12,25-diazatetracyclo[21.3.1.0(5,26).0(19,24)]heptacosa-1⁽²⁶⁾,2,4,19,21,23-hexaene-12-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

[(benzyloxycarbonyl)azanediyl]bis[(ethane-2,1-diyloxy)ethane-2,1-diyl] bis(4-methylbenzenesulfonate) (1315451-37-6) + 4,5-dihydroxyacridine-9(10H)-one (244184-94-9) → benzyl 27-oxo-6,9,15,18-tetraoxa-12,25-diazatetracyclo[21.3.1.0(5,26).0(19,24)]heptacosa-1(26),2,4,19,21,23-hexaene-12-carboxylate (1315451-39-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 72h; Inert atmosphere;

DOI:10.1016/j.tet.2011.05.050

Reference yield:

2,2'-{[(benzyloxycarbonyl)azanediyl]bis(ethane-2,1-diyloxy)}diethanol (254448-30-1) → benzyl 27-oxo-6,9,15,18-tetraoxa-12,25-diazatetracyclo[21.3.1.0(5,26).0(19,24)]heptacosa-1(26),2,4,19,21,23-hexaene-12-carboxylate (1315451-39-8)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / 24 h / 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 72 h / 50 °C / Inert atmosphere

With potassium carbonate; triethylamine; In N,N-dimethyl-formamide;

DOI:10.1016/j.tet.2011.05.050

Reference yield:

2,2'-((azanediylbis(ethane-2,1-diyl))bis(oxy))diethanol (54384-47-3) → benzyl 27-oxo-6,9,15,18-tetraoxa-12,25-diazatetracyclo[21.3.1.0(5,26).0(19,24)]heptacosa-1(26),2,4,19,21,23-hexaene-12-carboxylate (1315451-39-8)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / water / 6 h / 20 °C

2: triethylamine / 24 h / 20 °C / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 72 h / 50 °C / Inert atmosphere

With sodium hydrogencarbonate; potassium carbonate; triethylamine; In water; N,N-dimethyl-formamide;

DOI:10.1016/j.tet.2011.05.050

upstream raw materials:

2,2'-{[(benzyloxycarbonyl)azanediyl]bis(ethane-2,1-diyloxy)}diethanol

[(benzyloxycarbonyl)azanediyl]bis[(ethane-2,1-diyloxy)ethane-2,1-diyl] bis(4-methylbenzenesulfonate)

4,5-dihydroxyacridine-9(10H)-one

2,2'-((azanediylbis(ethane-2,1-diyl))bis(oxy))diethanol

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1315451-39-8 benzyl 27-oxo-6,9,15,18-tetraoxa-12,25-diazatetracyclo[21.3.1.0(5,26).0(19,24)]heptacosa-1⁽²⁶⁾,2,4,19,21,23-hexaene-12-carboxylate

Send

Send

Metric Ton KG G Pound L ML

Send

Send