4-methoxybenzyl 2,4-di-O-benzyl-3-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-α-L-rhamnopyranoside

Base Information

Chemical Name:4-methoxybenzyl 2,4-di-O-benzyl-3-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-α-L-rhamnopyranoside
CAS No.:172949-61-0
Molecular Formula:C₅₇H₅₇NO₁₄
Molecular Weight:980.078
Hs Code.:

Synonyms:4-methoxybenzyl 2,4-di-O-benzyl-3-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-α-L-rhamnopyranoside

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Chemical Property of 4-methoxybenzyl 2,4-di-O-benzyl-3-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-α-L-rhamnopyranoside

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Technology Process of 4-methoxybenzyl 2,4-di-O-benzyl-3-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-α-L-rhamnopyranoside

There total 4 articles about 4-methoxybenzyl 2,4-di-O-benzyl-3-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 128716-44-9
4-methoxybenzyl 2,4-di-O-benzyl-α-L-rhamnopyranoside

: 172949-61-0
4-methoxybenzyl 2,4-di-O-benzyl-3-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) silver aluminosilicate, molecular sieves 4 A / 1.) CH₂Cl₂, RT, 15 min, 2.) CH₂Cl₂, RT, 2.5 h

2: 1.) BH₃*THF / 1.) THF, a) -10 deg C, 0.5 h, b) RT, 2 h, 2.) THF, MeOH, RT, 1 h

With borane-THF; 4 A molecular sieve; silver aluminosilicate;
DOI:10.1248/cpb.43.1441

Reference yield:

: 141514-04-7
3,4,6-tri-O-benzoyl-2-benzoyloxyimino-α-D-arabino-hexopyranosyl iodide

: 172949-61-0
4-methoxybenzyl 2,4-di-O-benzyl-3-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / Ag₂CO₃ / CH₂Cl₂ / 4 h / Ambient temperature

2: 1.) BH₃*THF / 1.) THF, a) -10 deg C, 0.5 h, b) RT, 2 h, 2.) THF, MeOH, RT, 1 h

With borane-THF; silver carbonate; In dichloromethane;
DOI:10.1248/cpb.43.1441

Reference yield:

: 82469-72-5
3,4,6-tri-O-benzoyl-2-(benzoyloximino)-2-deoxy-α-D-arabino-hexopyranosyl bromide

: 172949-61-0
4-methoxybenzyl 2,4-di-O-benzyl-3-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) silver aluminosilicate, molecular sieves 4 A / 1.) CH₂Cl₂, RT, 15 min, 2.) CH₂Cl₂, RT, 2.5 h

2: 1.) BH₃*THF / 1.) THF, a) -10 deg C, 0.5 h, b) RT, 2 h, 2.) THF, MeOH, RT, 1 h

With borane-THF; 4 A molecular sieve; silver aluminosilicate;
DOI:10.1248/cpb.43.1441