3-N-methyl-N-[4'-[17β-hydroxy-3-oxo-17α-(1-propynyl)estra-4,9-dien-11β-yl]phenyl]aminopropionic acid

Base Information

Chemical Name:3-N-methyl-N-[4'-[17β-hydroxy-3-oxo-17α-(1-propynyl)estra-4,9-dien-11β-yl]phenyl]aminopropionic acid
CAS No.:1129547-79-0
Molecular Formula:C₃₁H₃₇NO₄
Molecular Weight:487.639
Hs Code.:

Synonyms:3-N-methyl-N-[4'-[17β-hydroxy-3-oxo-17α-(1-propynyl)estra-4,9-dien-11β-yl]phenyl]aminopropionic acid

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Chemical Property of 3-N-methyl-N-[4'-[17β-hydroxy-3-oxo-17α-(1-propynyl)estra-4,9-dien-11β-yl]phenyl]aminopropionic acid

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Technology Process of 3-N-methyl-N-[4'-[17β-hydroxy-3-oxo-17α-(1-propynyl)estra-4,9-dien-11β-yl]phenyl]aminopropionic acid

There total 1 articles about 3-N-methyl-N-[4'-[17β-hydroxy-3-oxo-17α-(1-propynyl)estra-4,9-dien-11β-yl]phenyl]aminopropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 590-92-1
3-Bromopropionic acid

: 104004-96-8
(8S,11R,13S,14S,17S)-17-hydroxy-13-methyl-11-(4-(methylamino)phenyl)-17-(prop-1-yn-1-yl)-1,2,6,7,8,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthren-3-one

: 1129547-79-0
3-N-methyl-N-[4'-[17β-hydroxy-3-oxo-17α-(1-propynyl)estra-4,9-dien-11β-yl]phenyl]aminopropionic acid

Guidance literature:: With sodium hydrogencarbonate; In ethanol; water; at 70 ℃; for 20h; pH=9.25;
DOI:10.1021/jm800985z

Reference yield:

: 1129547-79-0
3-N-methyl-N-[4'-[17β-hydroxy-3-oxo-17α-(1-propynyl)estra-4,9-dien-11β-yl]phenyl]aminopropionic acid

: C₃₆H₄₅NO₆

Guidance literature:: With triethylamine; isobutyl chloroformate; In tetrahydrofuran; at 0 ℃; for 0.666667h; Inert atmosphere;
DOI:10.1021/jm800985z