(S)-2-((3aR,5S,6S,6aR)-6-Benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-(4-methoxy-benzyloxy)-ethanethiol

Base Information

Chemical Name:(S)-2-((3aR,5S,6S,6aR)-6-Benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-(4-methoxy-benzyloxy)-ethanethiol
CAS No.:198995-06-1
Molecular Formula:C₂₄H₃₀O₆S
Molecular Weight:446.565
Hs Code.:

Synonyms:(S)-2-((3aR,5S,6S,6aR)-6-Benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-(4-methoxy-benzyloxy)-ethanethiol

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Chemical Property of (S)-2-((3aR,5S,6S,6aR)-6-Benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-(4-methoxy-benzyloxy)-ethanethiol

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Technology Process of (S)-2-((3aR,5S,6S,6aR)-6-Benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-(4-methoxy-benzyloxy)-ethanethiol

There total 5 articles about (S)-2-((3aR,5S,6S,6aR)-6-Benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-(4-methoxy-benzyloxy)-ethanethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22529-61-9
(1R)-1-((3aR,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro(2,3-d)(1,3)dioxol-5-yl)ethane-1,2-diol

: 198995-06-1
(S)-2-((3aR,5S,6S,6aR)-6-Benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-(4-methoxy-benzyloxy)-ethanethiol

Guidance literature:: Multi-step reaction with 3 steps

1: 41 percent / NaH / dimethylformamide

2: 88 percent / Ph₃P, DIAD

3: 70 percent / NaOH

With sodium hydroxide; di-isopropyl azodicarboxylate; sodium hydride; triphenylphosphine; In N,N-dimethyl-formamide;
DOI:10.1055/s-1997-990

Reference yield:

: 100-39-0
benzyl bromide

: 198995-06-1
(S)-2-((3aR,5S,6S,6aR)-6-Benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-(4-methoxy-benzyloxy)-ethanethiol

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / NaH / dimethylformamide / 5 h

2: 99 percent / 50percent aq. AcOH / 24 h / Ambient temperature

3: 41 percent / NaH / dimethylformamide

4: 88 percent / Ph₃P, DIAD

5: 70 percent / NaOH

With sodium hydroxide; di-isopropyl azodicarboxylate; sodium hydride; acetic acid; triphenylphosphine; In N,N-dimethyl-formamide;
DOI:10.1055/s-1997-990

Reference yield:

: 18685-18-2
3-O-benzyl-1,2-5,6-O-diisopropylidene-α-D-glucofuranose

: 198995-06-1
(S)-2-((3aR,5S,6S,6aR)-6-Benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-(4-methoxy-benzyloxy)-ethanethiol

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / 50percent aq. AcOH / 24 h / Ambient temperature

2: 41 percent / NaH / dimethylformamide

3: 88 percent / Ph₃P, DIAD

4: 70 percent / NaOH

With sodium hydroxide; di-isopropyl azodicarboxylate; sodium hydride; acetic acid; triphenylphosphine; In N,N-dimethyl-formamide;
DOI:10.1055/s-1997-990