N-methyl (2S,6S,7S,8R)-9,9-dimethyl-2-phenyl-1-aza-4-oxa[4.3.0^1,6]bicyclononan-5-one-7,8-dicarboximide

Base Information

• Chemical Name: N-methyl (2S,6S,7S,8R)-9,9-dimethyl-2-phenyl-1-aza-4-oxa[4.3.0^1,6]bicyclononan-5-one-7,8-dicarboximide
• CAS No.: 404891-54-9
• Molecular Formula: C₁₈H₂₀N₂O₄
• Molecular Weight: 328.368

Synonyms:N-methyl (2S,6S,7S,8R)-9,9-dimethyl-2-phenyl-1-aza-4-oxa[4.3.0^1,6]bicyclononan-5-one-7,8-dicarboximide

Chemical Property of N-methyl (2S,6S,7S,8R)-9,9-dimethyl-2-phenyl-1-aza-4-oxa[4.3.0^1,6]bicyclononan-5-one-7,8-dicarboximide

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Technology Process of N-methyl (2S,6S,7S,8R)-9,9-dimethyl-2-phenyl-1-aza-4-oxa[4.3.0^1,6]bicyclononan-5-one-7,8-dicarboximide

There total 2 articles about N-methyl (2S,6S,7S,8R)-9,9-dimethyl-2-phenyl-1-aza-4-oxa[4.3.0^1,6]bicyclononan-5-one-7,8-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

N-methylmaleimide (930-88-1) + (5S)-5-phenylmorpholin-2-one (144896-92-4,134872-85-8) + 2,2-dimethoxy-propane (77-76-9) → N-methyl (2S,6S,7S,8R)-9,9-dimethyl-2-phenyl-1-aza-4-oxa[4.3.01,6]bicyclononan-5-one-7,8-dicarboximide (404891-54-9)

Guidance literature:

With magnesium bromide; In tetrahydrofuran; for 6h;

DOI:10.1055/s-2006-939054

Reference yield: 33.0%

N-methylmaleimide (930-88-1) + (5S)-5-phenylmorpholin-2-one (144896-92-4,134872-85-8) + 2,2-dimethoxy-propane (77-76-9) → N-methyl (2S,6S,7S,8R)-9,9-dimethyl-2-phenyl-1-aza-4-oxa[4.3.01,6]bicyclononan-5-one-7,8-dicarboximide (404891-54-9) + (4S,6aS,9aR,9bS)-6,6,8-Trimethyl-4-phenyl-hexahydro-pyrrolo[3',4':3,4]pyrrolo[2,1-c][1,4]oxazine-1,7,9-trione

Guidance literature:

With magnesium bromide; In tetrahydrofuran; for 2.5h; Heating;

DOI:10.1055/s-2001-18762

upstream raw materials:

N-methylmaleimide

(5S)-5-phenylmorpholin-2-one

2,2-dimethoxy-propane

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