(R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid

Base Information

Chemical Name:(R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid
CAS No.:183665-62-5
Molecular Formula:C₁₈H₃₀N₂O₆
Molecular Weight:370.446
Hs Code.:

Synonyms:(R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid

Chemical Property:

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Technology Process of (R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid

There total 1 articles about (R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21568-87-6
2-aminocaprolactam

: 183665-62-5
(R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: dimethylsulfoxide

2: 1.) LiN(TMS)2 / 1.) THF, -78 deg C, 2.) THF

3: CF₃CO₂H

4: EDAC, HOBT

5: TFA

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; lithium hexamethyldisilazane; In dimethyl sulfoxide;
DOI:10.1016/S0960-894X(98)00370-9

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 183665-62-5
(R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid

: 183665-61-4
{(S)-3-[(R)-2-(Benzyloxycarbamoyl-methyl)-heptanoylamino]-2-oxo-azepan-1-yl}-acetic acid methyl ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
DOI:10.1016/S0960-894X(98)00370-9