N-(tert-butoxycarbonyl)-N-{[1-(ethyl 6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-α-L-erythro-hex-2-enopyranosid-4-yl)-1H-1,2,3-triazol-4-yl]methyl}-L-phenylalaninamide

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-N-{[1-(ethyl 6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-α-L-erythro-hex-2-enopyranosid-4-yl)-1H-1,2,3-triazol-4-yl]methyl}-L-phenylalaninamide
CAS No.:956107-03-2
Molecular Formula:C₃₁H₄₉N₅O₆Si
Molecular Weight:615.845
Hs Code.:

N-(tert-butoxycarbonyl)-N-{[1-(ethyl 6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-α-L-erythro-hex-2-enopyranosid-4-yl)-1H-1,2,3-triazol-4-yl]methyl}-L-phenylalaninamide

Synonyms:N-(tert-butoxycarbonyl)-N-{[1-(ethyl 6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-α-L-erythro-hex-2-enopyranosid-4-yl)-1H-1,2,3-triazol-4-yl]methyl}-L-phenylalaninamide

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Chemical Property of N-(tert-butoxycarbonyl)-N-{[1-(ethyl 6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-α-L-erythro-hex-2-enopyranosid-4-yl)-1H-1,2,3-triazol-4-yl]methyl}-L-phenylalaninamide

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Technology Process of N-(tert-butoxycarbonyl)-N-{[1-(ethyl 6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-α-L-erythro-hex-2-enopyranosid-4-yl)-1H-1,2,3-triazol-4-yl]methyl}-L-phenylalaninamide

There total 1 articles about N-(tert-butoxycarbonyl)-N-{[1-(ethyl 6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-α-L-erythro-hex-2-enopyranosid-4-yl)-1H-1,2,3-triazol-4-yl]methyl}-L-phenylalaninamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 864852-03-9
ethyl 4-azido-6-O-(tert-butyldimethylsilyl)-2,3,4-trideoxy-α-D-erythro-hex-2-enopyranoside

: 461638-99-3
(S)-tert-butyl (1-oxo-3-phenyl-1-(prop-2-yn-1-ylamino)propan-2-yl)carbamate

: 956107-03-2
N-(tert-butoxycarbonyl)-N-{[1-(ethyl 6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-α-L-erythro-hex-2-enopyranosid-4-yl)-1H-1,2,3-triazol-4-yl]methyl}-L-phenylalaninamide

Guidance literature:: With copper diacetate; sodium L-ascorbate; In tetrahydrofuran; water; tert-butyl alcohol; at 20 ℃;
DOI:10.1055/s-2007-983813

Reference yield:

: 956107-03-2
N-(tert-butoxycarbonyl)-N-{[1-(ethyl 6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-α-L-erythro-hex-2-enopyranosid-4-yl)-1H-1,2,3-triazol-4-yl]methyl}-L-phenylalaninamide

: C₃₁H₅₁N₅O₈Si

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; at 20 ℃;
DOI:10.1055/s-2007-983813

Reference yield:

: 956107-03-2
N-(tert-butoxycarbonyl)-N-{[1-(ethyl 6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-α-L-erythro-hex-2-enopyranosid-4-yl)-1H-1,2,3-triazol-4-yl]methyl}-L-phenylalaninamide

: N-(tert-butoxycarbonyl)-N-{[1-(ethyl 6-O-tert-butyldimethylsilyl-2,3-di-O-acetyl-4-deoxy-α-D-mannopyranosid-4-yl)-1H-1,2,3-triazol-4-yl]methyl}-L-phenylalaninamide

Guidance literature:: Multi-step reaction with 2 steps

1: OsO₄; N-methylmorpholine-N-oxide / acetone; H₂O / 20 °C

2: 231 mg / pyridine / 24 h / 20 °C

With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In pyridine; water; acetone;
DOI:10.1055/s-2007-983813