O²-(2,4-dinitro-5-fluorophenyl) 1-(N,N-dimethylamino)diazen-1-ium-1,2-diolate

Base Information

• Chemical Name: O²-(2,4-dinitro-5-fluorophenyl) 1-(N,N-dimethylamino)diazen-1-ium-1,2-diolate
• CAS No.: 903568-91-2
• Molecular Formula: C₈H₈FN₅O₆
• Molecular Weight: 289.18

Synonyms:O²-(2,4-dinitro-5-fluorophenyl) 1-(N,N-dimethylamino)diazen-1-ium-1,2-diolate

Chemical Property of O²-(2,4-dinitro-5-fluorophenyl) 1-(N,N-dimethylamino)diazen-1-ium-1,2-diolate

Chemical Property:

Purity/Quality:

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Technology Process of O²-(2,4-dinitro-5-fluorophenyl) 1-(N,N-dimethylamino)diazen-1-ium-1,2-diolate

There total 2 articles about O²-(2,4-dinitro-5-fluorophenyl) 1-(N,N-dimethylamino)diazen-1-ium-1,2-diolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-hydroxy-3,3-dimethyltriaz-1-ene 2-oxide sodium salt + 1,5-difluoro-2,4-dinitrobenzene (327-92-4) → O2-(2,4-dinitro-5-fluorophenyl) 1-(N,N-dimethylamino)diazen-1-ium-1,2-diolate (903568-91-2)

Guidance literature:

With sodium hydrogencarbonate; In tert-butyl alcohol;

DOI:10.1021/jm800831y

Reference yield:

1,5-difluoro-2,4-dinitrobenzene (327-92-4) + sodium 1-(N,N-dimethylamino)diazen-1-ium-1,2-diolate → O2-(2,4-dinitro-5-fluorophenyl) 1-(N,N-dimethylamino)diazen-1-ium-1,2-diolate (903568-91-2)

Guidance literature:

DOI:10.1021/jo0016529

Reference yield: 95.0%

sodium 1-[4-(n-propoxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate + O2-(2,4-dinitro-5-fluorophenyl) 1-(N,N-dimethylamino)diazen-1-ium-1,2-diolate (903568-91-2) → 1-[1-(N,N-dimethylamino)diazen-1-ium-1,2-diol-2-ato]-2,4-dinitro-5-{[(4-n-propoxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diol-2-ato}benzene (1093077-83-8)

Guidance literature:

In acetone; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/jm800831y

upstream raw materials:

1,5-difluoro-2,4-dinitrobenzene

Downstream raw materials:

O²-(2,4-dinitro-5-hydroxyphenyl) 1-(N,N-dimethylamino)diazen-1-ium-1,2-diolate

C₁₅H₁₆N₆O₇

O²-(2,4-dinitro-5-(4-(acetamido)phenoxy)) 1-(N,N-dimethylamino)diazen-1-ium-1,2-diolate

C₁₇H₁₈N₆O₈

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