N-2-(2-iodo-4,5-dimethoxyphenyl)ethyl-tert-butoxycarbonylacetamide

Base Information

Chemical Name:N-2-(2-iodo-4,5-dimethoxyphenyl)ethyl-tert-butoxycarbonylacetamide
CAS No.:1384186-28-0
Molecular Formula:C₁₇H₂₄INO₅
Molecular Weight:449.286
Hs Code.:

Synonyms:N-2-(2-iodo-4,5-dimethoxyphenyl)ethyl-tert-butoxycarbonylacetamide

Suppliers and Price of N-2-(2-iodo-4,5-dimethoxyphenyl)ethyl-tert-butoxycarbonylacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-2-(2-iodo-4,5-dimethoxyphenyl)ethyl-tert-butoxycarbonylacetamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-2-(2-iodo-4,5-dimethoxyphenyl)ethyl-tert-butoxycarbonylacetamide

There total 3 articles about N-2-(2-iodo-4,5-dimethoxyphenyl)ethyl-tert-butoxycarbonylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 66384-45-0
N-acetyl-2-iodo-4,5-dimethoxy-β-phenethylamine

: 1384186-28-0
N-2-(2-iodo-4,5-dimethoxyphenyl)ethyl-tert-butoxycarbonylacetamide

Guidance literature:: With dmap; In acetonitrile; at 20 ℃;
DOI:10.1021/ol301612q

Reference yield:

: 6275-29-2
N-[2-(3,4-dimethoxyphenyl)ethyl]acetamide

: 1384186-28-0
N-2-(2-iodo-4,5-dimethoxyphenyl)ethyl-tert-butoxycarbonylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: Iodine monochloride; acetic acid / 3 h / 20 °C

2: dmap / acetonitrile / 20 °C

With dmap; Iodine monochloride; acetic acid; In acetonitrile;
DOI:10.1021/ol301612q

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 1384186-28-0
N-2-(2-iodo-4,5-dimethoxyphenyl)ethyl-tert-butoxycarbonylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: Iodine monochloride; acetic acid / 3 h / 20 °C

3: dmap / acetonitrile / 20 °C

With dmap; Iodine monochloride; acetic acid; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/ol301612q