C₃₃H₄₁FN₂O₆

Base Information

Chemical Name:C₃₃H₄₁FN₂O₆
CAS No.:1335557-66-8
Molecular Formula:C₃₃H₄₁FN₂O₆
Molecular Weight:580.697
Hs Code.:

C<sub>33</sub>H<sub>41</sub>FN<sub>2</sub>O<sub>6</sub>

Synonyms:C₃₃H₄₁FN₂O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₄₁FN₂O₆

Chemical Property:

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Technology Process of C₃₃H₄₁FN₂O₆

There total 9 articles about C₃₃H₄₁FN₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7533-40-6,16369-17-8,53448-09-2,502-32-9,14438-11-0
2-amino-4-methyl-1-pentanol

: 1254339-82-6
C₂₇H₂₆FNO₆

: 1335557-66-8
C₃₃H₄₁FN₂O₆

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 1h;

Reference yield:

: 220901-72-4
3-fluoro-6-methoxy-2-methylbenzoic acid

: 1335557-66-8
C₃₃H₄₁FN₂O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 25 °C

1.2: 12 h / 25 °C

2.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

3.1: nitric acid; tetrabutylammomium bromide / water; 1,2-dichloro-ethane / 19 h / 20 - 26 °C

4.1: potassium carbonate; potassium iodide / acetone / 20 - 56 °C

5.1: water; sodium dithionite / tetrahydrofuran / 10 - 20.4 °C

6.1: dmap; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

7.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 0.58 h / -78 °C

7.2: 0.5 h / -78 °C

7.3: -78 - 20 °C

8.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1 h / 20 °C

With dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; tetrabutylammomium bromide; water; nitric acid; boron tribromide; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; diisopropylamine; N-ethyl-N,N-diisopropylamine; potassium iodide; In tetrahydrofuran; hexane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 394-04-7
5-fluoro-2-methoxybenzoic acid

: 1335557-66-8
C₃₃H₄₁FN₂O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran / 2 h / -78 °C

1.2: 2 h / -78 - 25 °C

2.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 25 °C

2.2: 12 h / 25 °C

3.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

4.1: nitric acid; tetrabutylammomium bromide / water; 1,2-dichloro-ethane / 19 h / 20 - 26 °C

5.1: potassium carbonate; potassium iodide / acetone / 20 - 56 °C

6.1: water; sodium dithionite / tetrahydrofuran / 10 - 20.4 °C

7.1: dmap; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

8.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 0.58 h / -78 °C

8.2: 0.5 h / -78 °C

8.3: -78 - 20 °C

9.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1 h / 20 °C

With dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; N,N,N,N,-tetramethylethylenediamine; tetrabutylammomium bromide; water; sec.-butyllithium; nitric acid; boron tribromide; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; diisopropylamine; N-ethyl-N,N-diisopropylamine; potassium iodide; In tetrahydrofuran; hexane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;