N,N'-1,3-propanediyl-bis[2-(benzyl-carbamoyl-methoxy)-benzamide]

Base Information

• Chemical Name: N,N'-1,3-propanediyl-bis[2-(benzyl-carbamoyl-methoxy)-benzamide]
• CAS No.: 935525-38-5
• Molecular Formula: C₃₅H₃₆N₄O₆
• Molecular Weight: 608.694
• Mol file: 935525-38-5.mol

Synonyms:N,N'-1,3-propanediyl-bis[2-(benzyl-carbamoyl-methoxy)-benzamide]

Chemical Property of N,N'-1,3-propanediyl-bis[2-(benzyl-carbamoyl-methoxy)-benzamide]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-1,3-propanediyl-bis[2-(benzyl-carbamoyl-methoxy)-benzamide]

There total 1 articles about N,N'-1,3-propanediyl-bis[2-(benzyl-carbamoyl-methoxy)-benzamide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

N-benzyl-2-chloroacetamide (2564-06-9) + N,N'-bis(2-hydroxybenzoyl)-1,3-diaminopropane (24350-74-1) → N,N'-1,3-propanediyl-bis[2-(benzyl-carbamoyl-methoxy)-benzamide] (935525-38-5)

Guidance literature:

With sodium hydroxide; In N,N-dimethyl-formamide; at 80 ℃; for 11h;

DOI:10.1016/j.saa.2006.04.040

Reference yield:

N,N'-1,3-propanediyl-bis[2-(benzyl-carbamoyl-methoxy)-benzamide] (935525-38-5) + water (7732-18-5) + dysprosium nitrate → [Dy(NO3)3(N,N'-1,3-propanediyl-bis[2-(benzylcarbamoylmethoxy)benzamide])]*2H2O

Guidance literature:

In chloroform; ethyl acetate; a soln. of metal nitrate in ethyl acetate was added to a soln. of benzamide-compound in chloroform, the mixt. was stirred for 8 h at room temp.; ppt. was sepd. by suction filtration, washed several times with ethyl acetate and chloroform, dried for 24 h in a vac. at room temp.; elem. anal.;

DOI:10.1016/j.saa.2006.04.040

Reference yield:

N,N'-1,3-propanediyl-bis[2-(benzyl-carbamoyl-methoxy)-benzamide] (935525-38-5) + water (7732-18-5) + terbium(III) picrate → [Tb2(picrate)6(N,N'-1,3-propanediyl-bis[2-(benzylcarbamoylmethoxy)benzamide])3]*4H2O

Guidance literature:

In chloroform; ethyl acetate; a soln. of metal picrate in ethyl acetate was added to a soln. of benzamide-compound in chloroform, the mixt. was stirred for 6 h at room temp.; diethyl ether was added, stirred for 4 h, ppt. was sepd. by suction filtration, washed several times with ethyl acetate, chloroform and diethyl ether, dried for 24 h in a vac. at room temp.; elem. anal.;

DOI:10.1016/j.saa.2006.04.040

upstream raw materials:

N-benzyl-2-chloroacetamide

N,N'-bis(2-hydroxybenzoyl)-1,3-diaminopropane