Technology Process of C27H30N2O
There total 4 articles about C27H30N2O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pivaloyl chloride;
In
dichloromethane;
at 0 - 20 ℃;
for 17h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / acetonitrile / 18 h / 20 - 60 °C / Inert atmosphere; Large scale
2.1: potassium trimethylsilonate / tetrahydrofuran / 16.33 h / 20 - 30 °C / Inert atmosphere; Large scale
2.2: 1 h / 0 - 20 °C / Inert atmosphere; Large scale
3.1: tetrahydrofuran; dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere; Large scale
With
potassium trimethylsilonate; potassium carbonate;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/op700073g
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / acetonitrile / 15.5 h / 20 - 50 °C / Inert atmosphere
2: tetrahydrofuran; dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere; Large scale
With
potassium carbonate;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/op700073g