5,6,11,12-tetrahydro-4-methoxy-1-phenylmethoxy-5,11-epoxydibenzo[a,c]cyclooctene

Base Information

Chemical Name:5,6,11,12-tetrahydro-4-methoxy-1-phenylmethoxy-5,11-epoxydibenzo[a,c]cyclooctene
CAS No.:391687-89-1
Molecular Formula:C₂₄H₂₂O₃
Molecular Weight:358.437
Hs Code.:

Synonyms:5,6,11,12-tetrahydro-4-methoxy-1-phenylmethoxy-5,11-epoxydibenzo[a,c]cyclooctene

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Chemical Property of 5,6,11,12-tetrahydro-4-methoxy-1-phenylmethoxy-5,11-epoxydibenzo[a,c]cyclooctene

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Technology Process of 5,6,11,12-tetrahydro-4-methoxy-1-phenylmethoxy-5,11-epoxydibenzo[a,c]cyclooctene

There total 8 articles about 5,6,11,12-tetrahydro-4-methoxy-1-phenylmethoxy-5,11-epoxydibenzo[a,c]cyclooctene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 391687-87-9
3,4-dihydro-3-methoxy-1-(2-phenylmethoxy-5-methoxyphenylmethyl)-1H-2-benzopyran

: 391687-89-1
5,6,11,12-tetrahydro-4-methoxy-1-phenylmethoxy-5,11-epoxydibenzo[a,c]cyclooctene

Guidance literature:: With tin(IV) chloride; In dichloromethane; at -78 ℃; for 0.25h;
DOI:10.1081/SCC-100106046

Reference yield:

: 391687-85-7
2-(2,2-dimethoxyethyl)-α-(2-phenylmethoxy-5-methoxyphenylmethyl)benzenemethanol

: 391687-89-1
5,6,11,12-tetrahydro-4-methoxy-1-phenylmethoxy-5,11-epoxydibenzo[a,c]cyclooctene

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / p-TsOH*H₂O / CH₂Cl₂ / 0.42 h / -78 - 20 °C

2: 89 percent / SnCl₄ / CH₂Cl₂ / 0.25 h / -78 °C

With tin(IV) chloride; toluene-4-sulfonic acid; In dichloromethane;
DOI:10.1081/SCC-100106046

Reference yield:

: 584-82-7
2-allyl-4-methoxyphenol

: 391687-89-1
5,6,11,12-tetrahydro-4-methoxy-1-phenylmethoxy-5,11-epoxydibenzo[a,c]cyclooctene

Guidance literature:: Multi-step reaction with 5 steps

1.1: O₃ / CH₂Cl₂ / 0.5 h / 0 °C

1.2: 0.31 g / PPh₃ / CH₂Cl₂ / 2.25 h / 0 - 20 °C

2.1: 72 percent / n-BuLi / tetrahydrofuran; hexane / 2 h / -78 - 20 °C

3.1: 96 percent / p-TsOH*H₂O / CH₂Cl₂ / 0.42 h / -78 - 20 °C

4.1: 89 percent / SnCl₄ / CH₂Cl₂ / 0.25 h / -78 °C

With n-butyllithium; tin(IV) chloride; toluene-4-sulfonic acid; ozone; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1081/SCC-100106046