2-Ethyl-5-chlot-2-phenyl-pentansaeurenitril

Base Information

• Chemical Name: 2-Ethyl-5-chlot-2-phenyl-pentansaeurenitril
• CAS No.: 1676-72-8
• Molecular Formula: C₁₃H₁₆ClN
• Molecular Weight: 221.73

Synonyms:2-Ethyl-5-chlot-2-phenyl-pentansaeurenitril

Chemical Property of 2-Ethyl-5-chlot-2-phenyl-pentansaeurenitril

Chemical Property:

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Technology Process of 2-Ethyl-5-chlot-2-phenyl-pentansaeurenitril

There total 4 articles about 2-Ethyl-5-chlot-2-phenyl-pentansaeurenitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-iodo-3-chloro-propane (6940-76-7) + 2-phenylbutanenitrile (769-68-6) → 2-Ethyl-5-chlot-2-phenyl-pentansaeurenitril (1676-72-8)

Guidance literature:

With lithium diisopropyl amide; In tetrahydrofuran; cyclohexane; at -78 - 20 ℃; for 1h;

DOI:10.1021/jm990316l

Reference yield:

2-phenylbutanenitrile (769-68-6) + 1.3-chlorobromopropane (109-70-6) → 2-Ethyl-5-chlot-2-phenyl-pentansaeurenitril (1676-72-8)

Guidance literature:

Multistep reaction; (i) LiNEt₂, (ii) /BRN= 605278/;

DOI:10.1139/v65-344

Reference yield:

2-phenylbutanenitrile (769-68-6) + 1.3-chlorobromopropane (109-70-6) → opt.inakt. 2,6-Diethyl-2,6-diphenyl-heptandisaeuredinitril (5298-51-1) + 2-Ethyl-5-chlot-2-phenyl-pentansaeurenitril (1676-72-8)

Guidance literature:

Multistep reaction; (i) NaNH₂, dioxane, (ii) /BRN= 605278/;

upstream raw materials:

2-phenylbutanenitrile

1.3-chlorobromopropane

1-iodo-3-chloro-propane

Downstream raw materials:

5-Cyan-2-aethyl-2-phenyl-cyclopentan-3-on

3-ethyl-2-amino-3-phenyl-cyclopent-1-enecarbonitrile

2-ethyl-2-phenyl-adiponitrile

2-Aethyl-2-phenyl-adipinsaeure-1-nitril

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