(2S)-methyl-2-[(2S,4R)-4-(benzyloxy)-2-(dimethoxyethyl)pyrrolidin-1-yl]-2-[(R)-2,2-dimethyl-1,3-dioxolan-4-yl]acetate

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Chemical Name:(2S)-methyl-2-[(2S,4R)-4-(benzyloxy)-2-(dimethoxyethyl)pyrrolidin-1-yl]-2-[(R)-2,2-dimethyl-1,3-dioxolan-4-yl]acetate
CAS No.:1189757-14-9
Molecular Formula:C₂₂H₃₃NO₇
Molecular Weight:423.507
Hs Code.:

Synonyms:(2S)-methyl-2-[(2S,4R)-4-(benzyloxy)-2-(dimethoxyethyl)pyrrolidin-1-yl]-2-[(R)-2,2-dimethyl-1,3-dioxolan-4-yl]acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-methyl-2-[(2S,4R)-4-(benzyloxy)-2-(dimethoxyethyl)pyrrolidin-1-yl]-2-[(R)-2,2-dimethyl-1,3-dioxolan-4-yl]acetate

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Technology Process of (2S)-methyl-2-[(2S,4R)-4-(benzyloxy)-2-(dimethoxyethyl)pyrrolidin-1-yl]-2-[(R)-2,2-dimethyl-1,3-dioxolan-4-yl]acetate

There total 1 articles about (2S)-methyl-2-[(2S,4R)-4-(benzyloxy)-2-(dimethoxyethyl)pyrrolidin-1-yl]-2-[(R)-2,2-dimethyl-1,3-dioxolan-4-yl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 755729-83-0
(2S,4R)-4-benzyloxy-2-dimethoxymethyl-pyrrolidine

: 917017-23-3
methyl(S)-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl](trifluoromethylsulfonyloxy)acetate

: 1189757-14-9
(2S)-methyl-2-[(2S,4R)-4-(benzyloxy)-2-(dimethoxyethyl)pyrrolidin-1-yl]-2-[(R)-2,2-dimethyl-1,3-dioxolan-4-yl]acetate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1002/chem.200900744

Reference yield:

: 1189757-14-9
(2S)-methyl-2-[(2S,4R)-4-(benzyloxy)-2-(dimethoxyethyl)pyrrolidin-1-yl]-2-[(R)-2,2-dimethyl-1,3-dioxolan-4-yl]acetate

: 1189757-17-2
(3aR,5aS,7R,9aS)-7-(benzyloxy)-5-methoxyoctahydro-1H-furo[3,4-b]pyrrolo[1,2-d][1,4]oxazin-1-one

: C₁₇H₂₁NO₅

Guidance literature:: With thionyl chloride; In methanol; for 4h; optical yield given as %de; Inert atmosphere; Reflux;
DOI:10.1002/chem.200900744