dithiocarbonic acid S-[3-(acetyl-allyl-amino)-2-methyl-3-oxo-1-phenyl-propyl] ester O-ethyl ester

Base Information

Chemical Name:dithiocarbonic acid S-[3-(acetyl-allyl-amino)-2-methyl-3-oxo-1-phenyl-propyl] ester O-ethyl ester
CAS No.:934192-59-3
Molecular Formula:C₁₈H₂₃NO₃S₂
Molecular Weight:365.518
Hs Code.:

dithiocarbonic acid <i>S</i>-[3-(acetyl-allyl-amino)-2-methyl-3-oxo-1-phenyl-propyl] ester <i>O</i>-ethyl ester

Synonyms:dithiocarbonic acid S-[3-(acetyl-allyl-amino)-2-methyl-3-oxo-1-phenyl-propyl] ester O-ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dithiocarbonic acid S-[3-(acetyl-allyl-amino)-2-methyl-3-oxo-1-phenyl-propyl] ester O-ethyl ester

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Technology Process of dithiocarbonic acid S-[3-(acetyl-allyl-amino)-2-methyl-3-oxo-1-phenyl-propyl] ester O-ethyl ester

There total 4 articles about dithiocarbonic acid S-[3-(acetyl-allyl-amino)-2-methyl-3-oxo-1-phenyl-propyl] ester O-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: N-allyl-N-(2-methyl-3-phenyl-acryloyl)-acetamide

: 140-89-6
potassium ethyl xanthogenate

: 934192-59-3
dithiocarbonic acid S-[3-(acetyl-allyl-amino)-2-methyl-3-oxo-1-phenyl-propyl] ester O-ethyl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 3h; Heating;

Reference yield:

: 1895-97-2
2-methyl-3-phenylacrylic acid

: 934192-59-3
dithiocarbonic acid S-[3-(acetyl-allyl-amino)-2-methyl-3-oxo-1-phenyl-propyl] ester O-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: SOCl₂ / 2 h / 20 °C

2.1: TEA; DMAP / petroleum ether / 15 h / 20 °C

3.1: NaH / tetrahydrofuran / 4 h / Heating

3.2: 69 percent / tetrahydrofuran / 4 h / Heating

4.1: 36 percent / TFA / CH₂Cl₂ / 3 h / Heating

With dmap; thionyl chloride; TEA; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; Petroleum ether;

Reference yield:

: 35086-87-4,38449-13-7
(E)-2-methyl-3-phenylacryloyl chloride

: 934192-59-3
dithiocarbonic acid S-[3-(acetyl-allyl-amino)-2-methyl-3-oxo-1-phenyl-propyl] ester O-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: TEA; DMAP / petroleum ether / 15 h / 20 °C

2.1: NaH / tetrahydrofuran / 4 h / Heating

2.2: 69 percent / tetrahydrofuran / 4 h / Heating

3.1: 36 percent / TFA / CH₂Cl₂ / 3 h / Heating

With dmap; TEA; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; Petroleum ether;