(2R,3S,4S,5R)-N-benzyl-2,3,4,6-tetrabenzyloxy-5-triethylsiloxyhexanamide

Base Information

Chemical Name:(2R,3S,4S,5R)-N-benzyl-2,3,4,6-tetrabenzyloxy-5-triethylsiloxyhexanamide
CAS No.:1414930-52-1
Molecular Formula:C₄₇H₅₇NO₆Si
Molecular Weight:760.058
Hs Code.:

Synonyms:(2R,3S,4S,5R)-N-benzyl-2,3,4,6-tetrabenzyloxy-5-triethylsiloxyhexanamide

Suppliers and Price of (2R,3S,4S,5R)-N-benzyl-2,3,4,6-tetrabenzyloxy-5-triethylsiloxyhexanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S,4S,5R)-N-benzyl-2,3,4,6-tetrabenzyloxy-5-triethylsiloxyhexanamide

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Technology Process of (2R,3S,4S,5R)-N-benzyl-2,3,4,6-tetrabenzyloxy-5-triethylsiloxyhexanamide

There total 3 articles about (2R,3S,4S,5R)-N-benzyl-2,3,4,6-tetrabenzyloxy-5-triethylsiloxyhexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 994-30-9
triethylsilyl chloride

: 1414930-60-1
(2R,3S,4S,5R)-N-benzyl-5-hydroxy-2,3,4,6-tetrabenzyloxyhexanamide

: 1414930-52-1
(2R,3S,4S,5R)-N-benzyl-2,3,4,6-tetrabenzyloxy-5-triethylsiloxyhexanamide

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 - 60 ℃; for 3h;
DOI:10.1016/j.tetlet.2012.10.042

Reference yield:

: 6386-24-9
2,3,4,6-tetra-O-benzyl-D-galactopyranose

: 1414930-52-1
(2R,3S,4S,5R)-N-benzyl-2,3,4,6-tetrabenzyloxy-5-triethylsiloxyhexanamide

Guidance literature:: Multi-step reaction with 3 steps

1: dimethyl sulfoxide / acetic anhydride / 8 h / 20 °C

2: toluene / 12 h / Reflux

3: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 - 60 °C

With 1H-imidazole; dimethyl sulfoxide; In acetic anhydride; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetlet.2012.10.042

Reference yield:

: 82598-84-3
2,3,4,6-tetra-O-benzyl-D-galactonolactone

: 1414930-52-1
(2R,3S,4S,5R)-N-benzyl-2,3,4,6-tetrabenzyloxy-5-triethylsiloxyhexanamide

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 12 h / Reflux

2: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 - 60 °C

With 1H-imidazole; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetlet.2012.10.042