benzyl 3-O-allyl-4-O-benzyl-2-deoxy-6-O-{2-deoxy-4,6-di-O-benzylidene-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl}-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

Base Information

Chemical Name:benzyl 3-O-allyl-4-O-benzyl-2-deoxy-6-O-{2-deoxy-4,6-di-O-benzylidene-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl}-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside
CAS No.:339317-03-2
Molecular Formula:C₉₅H₁₄₉Cl₃N₂O₁₇
Molecular Weight:1697.59
Hs Code.:

benzyl 3-O-allyl-4-O-benzyl-2-deoxy-6-O-{2-deoxy-4,6-di-O-benzylidene-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl}-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

Synonyms:benzyl 3-O-allyl-4-O-benzyl-2-deoxy-6-O-{2-deoxy-4,6-di-O-benzylidene-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl}-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

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Chemical Property of benzyl 3-O-allyl-4-O-benzyl-2-deoxy-6-O-{2-deoxy-4,6-di-O-benzylidene-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl}-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

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Technology Process of benzyl 3-O-allyl-4-O-benzyl-2-deoxy-6-O-{2-deoxy-4,6-di-O-benzylidene-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl}-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

There total 1 articles about benzyl 3-O-allyl-4-O-benzyl-2-deoxy-6-O-{2-deoxy-4,6-di-O-benzylidene-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl}-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 339317-01-0
benzyl 3-O-allyl-4-O-benzyl-2-deoxy-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

: 339316-81-3
2-deoxy-4,6-di-O-benzylidene-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranosyl trichloroacetimidate

: 339317-03-2
benzyl 3-O-allyl-4-O-benzyl-2-deoxy-6-O-{2-deoxy-4,6-di-O-benzylidene-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl}-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

Guidance literature:: With trifluoroborane diethyl ether; In dichloromethane; for 1h;
DOI:10.1016/j.carres.2007.01.012

Reference yield: 100.0%

: 339317-03-2
benzyl 3-O-allyl-4-O-benzyl-2-deoxy-6-O-{2-deoxy-4,6-di-O-benzylidene-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl}-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

: C₉₂H₁₄₈N₂O₁₅

Guidance literature:: With zinc; In acetic acid; ethyl acetate; at 20 ℃; for 24h;
DOI:10.1016/j.carres.2007.01.012

Reference yield: 62.0%

: 339317-03-2
benzyl 3-O-allyl-4-O-benzyl-2-deoxy-6-O-{2-deoxy-4,6-di-O-benzylidene-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl}-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

: benzyl 4-O-benzyl-2-deoxy-6-O-{2-deoxy-4,6-di-O-benzylidene-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl}-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

Guidance literature:: benzyl 3-O-allyl-4-O-benzyl-2-deoxy-6-O-{2-deoxy-4,6-di-O-benzylidene-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl}-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside; With hydrogen; In tetrahydrofuran; at 20 ℃; for 2h;

With N-Bromosuccinimide; water; In tetrahydrofuran; at 20 ℃; for 1h; Further stages.;
DOI:10.1016/j.carres.2007.01.012