benzyl 3-O-allyl-4-O-benzyl-2-deoxy-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

Base Information

Chemical Name:benzyl 3-O-allyl-4-O-benzyl-2-deoxy-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside
CAS No.:339317-01-0
Molecular Formula:C₅₁H₈₁NO₈
Molecular Weight:836.206
Hs Code.:

Synonyms:benzyl 3-O-allyl-4-O-benzyl-2-deoxy-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

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Chemical Property of benzyl 3-O-allyl-4-O-benzyl-2-deoxy-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

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Technology Process of benzyl 3-O-allyl-4-O-benzyl-2-deoxy-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

There total 6 articles about benzyl 3-O-allyl-4-O-benzyl-2-deoxy-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 339317-45-2
C₃₁H₂₉NO₇

: 339317-01-0
benzyl 3-O-allyl-4-O-benzyl-2-deoxy-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 95 percent / acetic acid; water / 6 h / 65 °C

2: 79 percent / DMAP; pyridine / 24 h / 20 - 40 °C

3: 57 percent / sodium hydride / dimethylformamide / 3 h / 20 °C

4: 87 percent / acetic acid; water / 1 h / 110 °C

5: 77 percent / hydrazine monohydrate / aq. ethanol / 2 h / Heating

6: 80 percent / DCC / CH₂Cl₂ / 24 h / 20 °C

With pyridine; dmap; water; sodium hydride; hydrazine hydrate; acetic acid; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2007.01.012

Reference yield:

: 339317-46-3
C₂₄H₂₅NO₇

: 339317-01-0
benzyl 3-O-allyl-4-O-benzyl-2-deoxy-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 79 percent / DMAP; pyridine / 24 h / 20 - 40 °C

2: 57 percent / sodium hydride / dimethylformamide / 3 h / 20 °C

3: 87 percent / acetic acid; water / 1 h / 110 °C

4: 77 percent / hydrazine monohydrate / aq. ethanol / 2 h / Heating

5: 80 percent / DCC / CH₂Cl₂ / 24 h / 20 °C

With pyridine; dmap; water; sodium hydride; hydrazine hydrate; acetic acid; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2007.01.012

Reference yield:

: 339316-98-2
benzyl 3-O-allyl-4-O-benzyl-2-deoxy-6-O-triphenylmethyl-2-phthalimido-β-D-glucopyranoside

: 339317-01-0
benzyl 3-O-allyl-4-O-benzyl-2-deoxy-2-[(R)-3-tetradecanoyloxytetradecanamido]-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / acetic acid; water / 1 h / 110 °C

2: 77 percent / hydrazine monohydrate / aq. ethanol / 2 h / Heating

3: 80 percent / DCC / CH₂Cl₂ / 24 h / 20 °C

With water; hydrazine hydrate; acetic acid; dicyclohexyl-carbodiimide; In ethanol; dichloromethane;
DOI:10.1016/j.carres.2007.01.012