phenyl (3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl (3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside
CAS No.:1361481-70-0
Molecular Formula:C₈₁H₈₁NO₁₅S
Molecular Weight:1340.6
Hs Code.:

phenyl (3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Synonyms:phenyl (3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Chemical Property of phenyl (3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Technology Process of phenyl (3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

There total 1 articles about phenyl (3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1361481-69-7
phenyl (2-O-acetyl-3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 1361481-70-0
phenyl (3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: phenyl (2-O-acetyl-3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside; With magnesium methanolate; In dichloromethane; at 20 ℃; for 72h; Inert atmosphere;

With acetic acid; In dichloromethane; pH=7;
DOI:10.1002/ejoc.201101062

Reference yield: 93.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1361481-70-0
phenyl (3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 74-88-4
methyl iodide

: 1361481-71-1
phenyl (3,4,6-tri-O-benzyl-2-O-(methylthio)thiocarbonyl-β-D-galactopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: phenyl (3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside; With 1H-imidazole; sodium hydride; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

carbon disulfide; In tetrahydrofuran; for 0.333333h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.201101062