2-iodo-3,4-dimethyl-1-nitrobenzene

Base Information

Chemical Name:2-iodo-3,4-dimethyl-1-nitrobenzene
CAS No.:909135-23-5
Molecular Formula:C₈H₈INO₂
Molecular Weight:277.062
Hs Code.:

Synonyms:2-iodo-3,4-dimethyl-1-nitrobenzene

Suppliers and Price of 2-iodo-3,4-dimethyl-1-nitrobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 2-iodo-3,4-dimethyl-1-nitrobenzene

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 2-iodo-3,4-dimethyl-1-nitrobenzene

There total 1 articles about 2-iodo-3,4-dimethyl-1-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 59146-96-2
2,3-dimethyl-6-nitroaniline

: 909135-23-5
2-iodo-3,4-dimethyl-1-nitrobenzene

Guidance literature:: 2,3-dimethyl-6-nitroaniline; With tert.-butylnitrite; methanesulfonic acid; In acetonitrile; at 20 ℃; for 0.25h;

With tetra-(n-butyl)ammonium iodide; In acetonitrile; at 20 ℃; for 4h;
DOI:10.1002/anie.202009395

Reference yield:

: 909135-23-5
2-iodo-3,4-dimethyl-1-nitrobenzene

: (S)-5,5',6,6'-tetramethyl-[1,1'-biphenyl]-2,2'-diamine

: C₃₂H₃₄N₄O₄

Guidance literature:: Multi-step reaction with 3 steps

1: copper / N,N-dimethyl-formamide / 11 h / 150 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 12 h / 20 °C / 750.08 Torr

3: (R)-3,3'-bis(2,4,6-triisopropylphenyl)binol phosphoric acid / chloroform / 85 h / -60 °C / Resolution of racemate

With (R)-3,3'-bis(2,4,6-triisopropylphenyl)binol phosphoric acid; palladium 10% on activated carbon; hydrogen; copper; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/anie.202009395

Reference yield:

: 909135-23-5
2-iodo-3,4-dimethyl-1-nitrobenzene

: 766-97-2
4-n-methylphenylacetylene

: 1,2-dimethyl-4-nitro-3-(p-tolylethynyl)benzene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In acetonitrile; at 70 ℃; for 0.441667h; Flow reactor;
DOI:10.1002/chem.201603626