1,1,3,3-tetramethyl-1,3-dihydrobenzo[c][1,2]oxasilole

Base Information

Chemical Name:1,1,3,3-tetramethyl-1,3-dihydrobenzo[c][1,2]oxasilole
CAS No.:1239384-07-6
Molecular Formula:C₁₁H₁₆OSi
Molecular Weight:192.333
Hs Code.:

Synonyms:1,1,3,3-tetramethyl-1,3-dihydrobenzo[c][1,2]oxasilole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1,3,3-tetramethyl-1,3-dihydrobenzo[c][1,2]oxasilole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,1,3,3-tetramethyl-1,3-dihydrobenzo[c][1,2]oxasilole

There total 26 articles about 1,1,3,3-tetramethyl-1,3-dihydrobenzo[c][1,2]oxasilole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 623-12-1
4-chloromethoxybenzene

: 1262886-86-1
C₁₇H₂₂OSi

: 613-37-6
4-methoxylbiphenyl

: 1239384-07-6
1,1,3,3-tetramethyl-1,3-dihydrobenzo[c][1,2]oxasilole

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; (1,2-dimethoxyethane)dichloronickel(II); caesium carbonate; zinc; tricyclohexylphosphine; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; at 20 - 80 ℃; for 30h; chemoselective reaction; Inert atmosphere;
DOI:10.1039/c0cc02173c

Reference yield:

: 5332-24-1
3-bromoquinoline

: 1239384-06-5
[2-(2-hydroxyprop-2-yl)phenyl]trimethylsilane

: 612-58-8
3-methylquinoline

: 1239384-07-6
1,1,3,3-tetramethyl-1,3-dihydrobenzo[c][1,2]oxasilole

Guidance literature:: With potassium phosphate; monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; palladium diacetate; In tetrahydrofuran; at 100 ℃; for 4h; Inert atmosphere;
DOI:10.1002/anie.201000816

Reference yield:

: 578-57-4
2-bromoanisole

: 1239384-06-5
[2-(2-hydroxyprop-2-yl)phenyl]trimethylsilane

: 578-58-5
2-methylmethoxybenzene

: 1239384-07-6
1,1,3,3-tetramethyl-1,3-dihydrobenzo[c][1,2]oxasilole

Guidance literature:: With potassium phosphate; monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; palladium diacetate; In tetrahydrofuran; at 100 ℃; for 18h; Inert atmosphere;
DOI:10.1002/anie.201000816