4-(Phenylsulfanylmethyl)-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

Base Information

Chemical Name:4-(Phenylsulfanylmethyl)-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion
CAS No.:286374-69-4
Molecular Formula:C₁₇H₁₂F₃NS₃
Molecular Weight:383.482
Hs Code.:

Synonyms:4-(Phenylsulfanylmethyl)-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

Suppliers and Price of 4-(Phenylsulfanylmethyl)-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(Phenylsulfanylmethyl)-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(Phenylsulfanylmethyl)-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

There total 4 articles about 4-(Phenylsulfanylmethyl)-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 108-98-5
thiophenol

: 286374-52-5
4-Chlormethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

: 286374-69-4
4-(Phenylsulfanylmethyl)-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In methanol; at 20 ℃; for 24h;

Reference yield:

: 98-16-8
3-trifluoromethylaniline

: 286374-69-4
4-(Phenylsulfanylmethyl)-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

Guidance literature:: Multi-step reaction with 4 steps

1: 30.12 g / 20 °C

2: 80 percent / methanol; acetone / 2 h / 20 °C

3: 22.08 g / HCl / ethyl acetate / 2 h / Heating

4: 83 percent / 1,4-diazabicyclo[2.2.2]octane / methanol / 24 h / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; hydrogenchloride; In methanol; ethyl acetate; acetone; 1: Addition / 2: Cyclization / 3: Dehydration / 4: Substitution;

Reference yield:

: 286374-46-7
4-Chlormethyl-4-hydroxy-3-(3-trifluormethylphenyl)-1,3-thiazolidin-2-thion

: 286374-69-4
4-(Phenylsulfanylmethyl)-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

Guidance literature:: Multi-step reaction with 2 steps

1: 22.08 g / HCl / ethyl acetate / 2 h / Heating

2: 83 percent / 1,4-diazabicyclo[2.2.2]octane / methanol / 24 h / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; hydrogenchloride; In methanol; ethyl acetate; 1: Dehydration / 2: Substitution;