(E)-2-(2,4-Dichloro-phenyl)-1-[1,2,4]triazol-1-yl-5-trimethylsilanyl-pent-4-en-2-ol

Base Information

• Chemical Name: (E)-2-(2,4-Dichloro-phenyl)-1-[1,2,4]triazol-1-yl-5-trimethylsilanyl-pent-4-en-2-ol
• CAS No.: 123871-87-4
• Molecular Formula: C₁₆H₂₁Cl₂N₃OSi
• Molecular Weight: 370.354

Synonyms:(E)-2-(2,4-Dichloro-phenyl)-1-[1,2,4]triazol-1-yl-5-trimethylsilanyl-pent-4-en-2-ol

Chemical Property of (E)-2-(2,4-Dichloro-phenyl)-1-[1,2,4]triazol-1-yl-5-trimethylsilanyl-pent-4-en-2-ol

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Technology Process of (E)-2-(2,4-Dichloro-phenyl)-1-[1,2,4]triazol-1-yl-5-trimethylsilanyl-pent-4-en-2-ol

There total 2 articles about (E)-2-(2,4-Dichloro-phenyl)-1-[1,2,4]triazol-1-yl-5-trimethylsilanyl-pent-4-en-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-3-bromo-1-(trimethylsilyl)propene (84673-88-1,87506-22-7) + 1-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-yl)ethanone (58905-16-1) → (E)-2-(2,4-Dichloro-phenyl)-1-[1,2,4]triazol-1-yl-5-trimethylsilanyl-pent-4-en-2-ol (123871-87-4)

Guidance literature:

With ethylene dibromide; zinc; Yield given. Multistep reaction; 1.) THF, 25-30 deg C; 2.) CH₂Cl₂, r.t., 15-16 h;

DOI:10.1016/0022-328X(89)80112-3

Reference yield:

(E)-3-bromo-1-(trimethylsilyl)propene (84673-88-1,87506-22-7) + 1-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-yl)ethanone (58905-16-1) → 2-(2,4-Dichloro-phenyl)-1-[1,2,4]triazol-1-yl-3-trimethylsilanyl-pent-4-en-2-ol + (E)-2-(2,4-Dichloro-phenyl)-1-[1,2,4]triazol-1-yl-5-trimethylsilanyl-pent-4-en-2-ol (123871-87-4)

Guidance literature:

With aluminium; Yield given. Multistep reaction. Yields of byproduct given; 1.) ether, reflux, 5h; 2.) CH₂Cl₂, r.t., 15-20 h;

DOI:10.1016/0022-328X(89)80112-3

Reference yield: 51.0%

(E)-2-(2,4-Dichloro-phenyl)-1-[1,2,4]triazol-1-yl-5-trimethylsilanyl-pent-4-en-2-ol (123871-87-4) → 2-(2,4-dichlorophenyl)-1-(1H-1,2,4-triazol-1-yl)-5-trimethylsilyl-2-pentanol

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 2h;

DOI:10.1016/0022-328X(89)80112-3

upstream raw materials:

(E)-3-bromo-1-(trimethylsilyl)propene

1-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-yl)ethanone

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