10-Hydroxy-1,10,11,11-tetramethyl-4-phenyl-2,4,6-triazatricyclo<5.3.1.0^2,6>undec-8-en-3,5-dion

Base Information

• Chemical Name: 10-Hydroxy-1,10,11,11-tetramethyl-4-phenyl-2,4,6-triazatricyclo<5.3.1.0^2,6>undec-8-en-3,5-dion
• CAS No.: 100084-57-9
• Molecular Formula: C₁₈H₂₁N₃O₃
• Molecular Weight: 327.383

Synonyms:10-Hydroxy-1,10,11,11-tetramethyl-4-phenyl-2,4,6-triazatricyclo<5.3.1.0^2,6>undec-8-en-3,5-dion

Chemical Property of 10-Hydroxy-1,10,11,11-tetramethyl-4-phenyl-2,4,6-triazatricyclo<5.3.1.0^2,6>undec-8-en-3,5-dion

Chemical Property:

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Technology Process of 10-Hydroxy-1,10,11,11-tetramethyl-4-phenyl-2,4,6-triazatricyclo<5.3.1.0^2,6>undec-8-en-3,5-dion

There total 2 articles about 10-Hydroxy-1,10,11,11-tetramethyl-4-phenyl-2,4,6-triazatricyclo<5.3.1.0^2,6>undec-8-en-3,5-dion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) → 10-Hydroxy-1,10,11,11-tetramethyl-4-phenyl-2,4,6-triazatricyclo<5.3.1.02,6>undec-8-en-3,5-dion (100084-57-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / benzene / 2 h / Heating

2: diethyl ether / 6 h / Heating

In diethyl ether; benzene;

Reference yield:

methyl magnesium iodide (917-64-6) + 1,11,11-Trimethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.02,6>undec-8-en-3,5,10-trion (100084-46-6) → 10-Hydroxy-1,10,11,11-tetramethyl-4-phenyl-2,4,6-triazatricyclo<5.3.1.02,6>undec-8-en-3,5-dion (100084-57-9) + (1S*,10R*)-10-Hydroxy-1,10,11,11-tetramethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.02,6>undec-8-en-3,5-dion (100084-55-7)

Guidance literature:

In diethyl ether; for 6h; Yield given. Yields of byproduct given; Heating;

Reference yield: 80.0%

10-Hydroxy-1,10,11,11-tetramethyl-4-phenyl-2,4,6-triazatricyclo<5.3.1.02,6>undec-8-en-3,5-dion (100084-57-9) → 1,11,11-Trimethyl-10-methylen-4-phenyl-2,4,6-triazatricyclo<5.3.1.02,6>undec-8-en-3,5-dion (100102-77-0)

Guidance literature:

With trichlorophosphate; In pyridine; for 24h; Heating;

upstream raw materials:

methyl magnesium iodide

1,11,11-Trimethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5,10-trion

4-Phenyl-1,2,4-triazolidine-3,5-dione

Downstream raw materials:

1,11,11-Trimethyl-10-methylen-4-phenyl-2,4,6-triazatricyclo<5.3.1.0^2,6>undec-8-en-3,5-dion

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