11-(4-methoxytritylamino)-N-{1-[4-(4-hyroxybutoxy)-3-methoxy-6-nitrophenyl]ethyl}undecanamide

Base Information

Chemical Name:11-(4-methoxytritylamino)-N-{1-[4-(4-hyroxybutoxy)-3-methoxy-6-nitrophenyl]ethyl}undecanamide
CAS No.:945495-94-3
Molecular Formula:C₄₄H₅₇N₃O₇
Molecular Weight:739.952
Hs Code.:

Synonyms:11-(4-methoxytritylamino)-N-{1-[4-(4-hyroxybutoxy)-3-methoxy-6-nitrophenyl]ethyl}undecanamide

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Chemical Property of 11-(4-methoxytritylamino)-N-{1-[4-(4-hyroxybutoxy)-3-methoxy-6-nitrophenyl]ethyl}undecanamide

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Technology Process of 11-(4-methoxytritylamino)-N-{1-[4-(4-hyroxybutoxy)-3-methoxy-6-nitrophenyl]ethyl}undecanamide

There total 4 articles about 11-(4-methoxytritylamino)-N-{1-[4-(4-hyroxybutoxy)-3-methoxy-6-nitrophenyl]ethyl}undecanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 252851-63-1
4-[4-(1-aminoethyl)-2-methoxy-5-nitrophenoxy]-1-butanol

: 135672-65-0
11-undecanoic acid

: 945495-94-3
11-(4-methoxytritylamino)-N-{1-[4-(4-hyroxybutoxy)-3-methoxy-6-nitrophenyl]ethyl}undecanamide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In pyridine; at 20 ℃; for 3h;
DOI:10.1039/b704587e

Reference yield:

: 945495-93-2
4-(2-methoxy-5-nitro-4-[1-(2,2,2-trifluoroacetamido)ethyl]phenoxy)butyl acetate

: 945495-94-3
11-(4-methoxytritylamino)-N-{1-[4-(4-hyroxybutoxy)-3-methoxy-6-nitrophenyl]ethyl}undecanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / NaOH / methanol / 6 h / Heating

2: 86 percent / EDC*HCl / pyridine / 3 h / 20 °C

With sodium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In pyridine; methanol;
DOI:10.1039/b704587e

Reference yield:

: 2432-99-7,25587-80-8,84029-94-7
11-aminoundecanoic acid

: 945495-94-3
11-(4-methoxytritylamino)-N-{1-[4-(4-hyroxybutoxy)-3-methoxy-6-nitrophenyl]ethyl}undecanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / pyridine / 3 h / 20 °C

2: 86 percent / EDC*HCl / pyridine / 3 h / 20 °C

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In pyridine;
DOI:10.1039/b704587e